2,3,7,8-bismethylenedioxy-6,11-dimethoxy-5-methyl-5,6-dihydrobenzophenanthridine

Base Information

Chemical Name:2,3,7,8-bismethylenedioxy-6,11-dimethoxy-5-methyl-5,6-dihydrobenzophenanthridine
CAS No.:98260-77-6
Molecular Formula:C₂₂H₁₉NO₆
Molecular Weight:393.396
Hs Code.:

2,3,7,8-bismethylenedioxy-6,11-dimethoxy-5-methyl-5,6-dihydrobenzo<c>phenanthridine

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3,7,8-bismethylenedioxy-6,11-dimethoxy-5-methyl-5,6-dihydrobenzophenanthridine

Chemical Property:

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Technology Process of 2,3,7,8-bismethylenedioxy-6,11-dimethoxy-5-methyl-5,6-dihydrobenzophenanthridine

There total 5 articles about 2,3,7,8-bismethylenedioxy-6,11-dimethoxy-5-methyl-5,6-dihydrobenzophenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 98260-75-4
2,3,7,8-bismethylenedioxy-11-methoxy-5-methyl-5,6-dihydrodibenzophenanthridine

: 98260-77-6
2,3,7,8-bismethylenedioxy-6,11-dimethoxy-5-methyl-5,6-dihydrobenzophenanthridine

Guidance literature:: With sodium hydroxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In benzene; for 2h;

Reference yield:

: 28342-27-0
2,3,7,8-bismethylenedioxy-11-methoxy-5-methyl-6-oxobenzophenanthridine

: 98260-77-6
2,3,7,8-bismethylenedioxy-6,11-dimethoxy-5-methyl-5,6-dihydrobenzophenanthridine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / LiAlH₄ / tetrahydrofuran / 6 h / Heating

2: 82 percent / dichlorodicyanobenzoquinone, aq. NaOH / benzene / 2 h

With sodium hydroxide; lithium aluminium tetrahydride; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; benzene;

Reference yield:

: 98260-84-5
N-(3-methoxy-6,7-methylenedioxynaphth-1-yl)-N-methylamide of 6-bromo-2,3-methylenedioxybenzoic acid

: 98260-77-6
2,3,7,8-bismethylenedioxy-6,11-dimethoxy-5-methyl-5,6-dihydrobenzophenanthridine

Guidance literature:: Multi-step reaction with 3 steps

1: 5.3 percent / triethylamine / acetonitrile / 12 h / Irradiation

2: 90 percent / LiAlH₄ / tetrahydrofuran / 6 h / Heating

3: 82 percent / dichlorodicyanobenzoquinone, aq. NaOH / benzene / 2 h

With sodium hydroxide; lithium aluminium tetrahydride; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; acetonitrile; benzene;