C₄₀H₅₅N₈O₁₄P

Base Information

Chemical Name:C₄₀H₅₅N₈O₁₄P
CAS No.:1435456-93-1
Molecular Formula:C₄₀H₅₅N₈O₁₄P
Molecular Weight:902.896
Hs Code.:

C<sub>40</sub>H<sub>55</sub>N<sub>8</sub>O<sub>14</sub>P

Synonyms:

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Chemical Property of C₄₀H₅₅N₈O₁₄P

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Technology Process of C₄₀H₅₅N₈O₁₄P

There total 9 articles about C₄₀H₅₅N₈O₁₄P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1435456-78-2
C₄₁H₆₇N₇O₁₁Si₂

: 1435456-93-1
C₄₀H₅₅N₈O₁₄P

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 15 h / 20 °C

2: tert-butylmagnesium chloride / tetrahydrofuran / 20 °C

With tert-butylmagnesium chloride; triethylamine tris(hydrogen fluoride); In tetrahydrofuran;
DOI:10.1016/j.bmcl.2013.03.077

Reference yield:

: C₁₉H₂₄N₆O₆

: 1435456-93-1
C₄₀H₅₅N₈O₁₄P

Guidance literature:: Multi-step reaction with 5 steps

1.1: ammonia / methanol / 24 h / 20 °C

1.2: 72 h / 20 °C

2.1: pyridine / 20 °C

3.1: dmap / 30 h / 20 °C

4.1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 15 h / 20 °C

5.1: tert-butylmagnesium chloride / tetrahydrofuran / 20 °C

With pyridine; dmap; tert-butylmagnesium chloride; ammonia; triethylamine tris(hydrogen fluoride); In tetrahydrofuran; methanol;
DOI:10.1016/j.bmcl.2013.03.077

Reference yield:

: 4-amino-6-bromo-5-cyano-1H-pyrrolo[2,3-d]pyrimidine

: 1435456-93-1
C₄₀H₅₅N₈O₁₄P

Guidance literature:: Multi-step reaction with 9 steps

1.1: N,O-bis-(trimethylsilyl)-acetamide / acetonitrile / 0.33 h / 20 °C

1.2: 3 h / 80 - 85 °C

2.1: ammonia / methanol

3.1: ammonia / 110 °C

4.1: 2 h / Reflux

5.1: ammonia / methanol / 24 h / 20 °C

5.2: 72 h / 20 °C

6.1: pyridine / 20 °C

7.1: dmap / 30 h / 20 °C

8.1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 15 h / 20 °C

9.1: tert-butylmagnesium chloride / tetrahydrofuran / 20 °C

With pyridine; dmap; N,O-bis-(trimethylsilyl)-acetamide; tert-butylmagnesium chloride; ammonia; triethylamine tris(hydrogen fluoride); In tetrahydrofuran; methanol; acetonitrile; 1.1: |Vorbrueggen Nucleoside Synthesis;
DOI:10.1016/j.bmcl.2013.03.077