2-Propenoic acid, 3-chloro-2-formyl-3-(4-nitrophenyl)-, methyl ester, (E)-

Base Information

Chemical Name:2-Propenoic acid, 3-chloro-2-formyl-3-(4-nitrophenyl)-, methyl ester, (E)-
CAS No.:106098-04-8
Molecular Formula:C₁₁H₈ClNO₅
Molecular Weight:269.641
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Propenoic acid, 3-chloro-2-formyl-3-(4-nitrophenyl)-, methyl ester, (E)-

Chemical Property:

Purity/Quality:

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Technology Process of 2-Propenoic acid, 3-chloro-2-formyl-3-(4-nitrophenyl)-, methyl ester, (E)-

There total 5 articles about 2-Propenoic acid, 3-chloro-2-formyl-3-(4-nitrophenyl)-, methyl ester, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 56377-30-1
Methyl (Z)-β-chloro-p-nitrocinnamate

: 106098-10-6
methyl (E)-β-chloro-p-nitrocinnamate

: 106098-04-8
(E)-β-chloro-α-(methoxycarbonyl)-p-nitrocinnamaldehyde

: 106098-08-2
(Z)-β-chloro-α-(methoxycarbonyl)-p-nitrocinnamaldehyde

Guidance literature:: With N,N-dimethyl-formamide; trichlorophosphate; In Trichloroethylene; at 95 ℃; for 20h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo00372a005

Reference yield:

: 838-57-3
ethyl 4-nitrobenzoylacetate

: 106098-04-8
(E)-β-chloro-α-(methoxycarbonyl)-p-nitrocinnamaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / conc. H₂SO₄ / 22 h / Heating

2: 1.) POCl₃ / 1.) trichloroethylene, 2.) trichlorethylene, 95 deg C, 20 h

With sulfuric acid; trichlorophosphate;
DOI:10.1021/jo00372a005

Reference yield:

: 59156-55-7
methyl 3-(4-nitrophenyl)-3-oxopropanoate

: 68-12-2,33513-42-7
N,N-dimethyl-formamide

: 106098-04-8
(E)-β-chloro-α-(methoxycarbonyl)-p-nitrocinnamaldehyde

: 106098-08-2
(Z)-β-chloro-α-(methoxycarbonyl)-p-nitrocinnamaldehyde

: 106098-09-3
(E)-β-chloro-α-(methoxycarbonyl)-p-nitrocinnamic acid

: 106098-17-3
(Z)-β-chloro-α-(methoxycarbonyl)-p-nitrocinnamic acid

Guidance literature:: With trichlorophosphate; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts; 1.) trichloroethylene, 2.) trichlorethylene, 95 deg C, 20 h;
DOI:10.1021/jo00372a005