(1S,18²S,18³S)-18²-(4-acetoxy-phenyl)-2,6-diacetyl-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione

Base Information

• Chemical Name: (1S,18²S,18³S)-18²-(4-acetoxy-phenyl)-2,6-diacetyl-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione
• CAS No.: 133162-93-3
• Molecular Formula: C₃₄H₄₂N₄O₇
• Molecular Weight: 618.73

Synonyms:

Chemical Property of (1S,18²S,18³S)-18²-(4-acetoxy-phenyl)-2,6-diacetyl-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (1S,18²S,18³S)-18²-(4-acetoxy-phenyl)-2,6-diacetyl-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione

There total 1 articles about (1S,18²S,18³S)-18²-(4-acetoxy-phenyl)-2,6-diacetyl-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S,182S,183S)-182-(4-hydroxy-phenyl)-182,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione (75363-58-5) + acetic anhydride (108-24-7) → (1S,182S,183S)-182-(4-acetoxy-phenyl)-2,6-diacetyl-182,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione (69755-30-2,71657-56-2,133162-93-3)

Guidance literature:

With pyridine;

DOI:10.1002/hlca.19780610735

Reference yield:

(1S,182S,183S)-182-(4-acetoxy-phenyl)-2,6-diacetyl-182,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione (69755-30-2,71657-56-2,133162-93-3) → (13R,13S)-8,12-diacetyl-3-(3-benzoylamino-propyl)-13-(2-hydroxy-ethyl)-12c-(4-methoxy-phenyl)-(13rH)-12,3-dihydro-3,8,12-triaza-1(3,5)-benzofurana-cyclotridecaphan-2-one (69721-76-2,73745-74-1)

Guidance literature:

Multi-step reaction with 6 steps

1: aq. NaOH

2: diethyl ether; methanol

3: pyridine

4: aq. NaOH

5: HCl

6: LiBH₄ / tetrahydrofuran

With hydrogenchloride; sodium hydroxide; lithium borohydride; In tetrahydrofuran; pyridine; methanol; diethyl ether;

DOI:10.1002/hlca.19780610735

Reference yield:

(1S,182S,183S)-182-(4-acetoxy-phenyl)-2,6-diacetyl-182,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione (69755-30-2,71657-56-2,133162-93-3) → [(13S,13S)-8,12-diacetyl-3-(3-benzoylamino-propyl)-12c-(4-methoxy-phenyl)-2-oxo-(13rH)-12,3-dihydro-3,8,12-triaza-1(3,5)-benzofurana-cyclotridecaphan-13-yl]-acetic acid (69721-73-9,73745-72-9)

Guidance literature:

Multi-step reaction with 4 steps

1: aq. NaOH

2: diethyl ether; methanol

3: pyridine

4: aq. NaOH

With sodium hydroxide; In pyridine; methanol; diethyl ether;

DOI:10.1002/hlca.19780610735

upstream raw materials:

(1S,18²S,18³S)-18²-(4-hydroxy-phenyl)-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione

acetic anhydride

Downstream raw materials:

(1S,18²S,18³S)-2,6-diacetyl-18²-(4-hydroxy-phenyl)-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione

(1S,18²S,18³S)-2,6-diacetyl-18²-(4-methoxy-phenyl)-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione

(1S,19³S)-2,6-diacetyl-15-benzoyl-18²c-(4-methoxy-phenyl)-(18³rH)-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]cyclononadecaphane-16,19-dione

(1³R,13S)-13-(2-acetoxy-ethyl)-8,12-diacetyl-3-(3-benzoylamino-propyl)-1²c-(4-methoxy-phenyl)-(1³rH)-1^2,3-dihydro-3,8,12-triaza-1(3,5)-benzofurana-cyclotridecaphan-2-one

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