1,2-Dihydro-2-oxo-N-phenyl-1-acenaphthylencarboxamid

Base Information

Chemical Name:1,2-Dihydro-2-oxo-N-phenyl-1-acenaphthylencarboxamid
CAS No.:81400-04-6
Molecular Formula:C₁₉H₁₃NO₂
Molecular Weight:287.318
Hs Code.:

Synonyms:

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Chemical Property of 1,2-Dihydro-2-oxo-N-phenyl-1-acenaphthylencarboxamid

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Technology Process of 1,2-Dihydro-2-oxo-N-phenyl-1-acenaphthylencarboxamid

There total 7 articles about 1,2-Dihydro-2-oxo-N-phenyl-1-acenaphthylencarboxamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 81400-02-4
3-Diazo-1H-phenalen-1,2(3H)-dion

: 62-53-3
aniline

: 81400-04-6
1,2-Dihydro-2-oxo-N-phenyl-1-acenaphthylencarboxamid

Guidance literature:: Heating;

Reference yield:

: 81400-03-5
phenalenedione

: 81400-04-6
1,2-Dihydro-2-oxo-N-phenyl-1-acenaphthylencarboxamid

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / TsN₃, KOEt / ethanol / 1) 2 h, 5 deg C, 2) 2 h, r.t.

2: 93 percent / Heating

With 4-toluenesulfonyl azide; potassium ethoxide; In ethanol;

Reference yield:

: 107396-76-9
2-Phenyl-4H-naphtho[1,8-cd]azepine-1,3-dione

: 81400-04-6
1,2-Dihydro-2-oxo-N-phenyl-1-acenaphthylencarboxamid

Guidance literature:: With hydrogenchloride; ethanol; sodium; Yield given. Multistep reaction; 1.) room temperature, 10 min, 2.) room temperature, 10 min;