Technology Process of C25H28O4
There total 10 articles about C25H28O4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dibromotriphenylphosphorane / acetonitrile
2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / water; 1,4-dioxane
3: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; tetrakis(triphenylphosphine) palladium(0); potassium acetate; sodium carbonate; dibromotriphenylphosphorane;
In
1,4-dioxane; water; toluene; acetonitrile;
2: |Miyaura Borylation Reaction;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: lithium diisopropyl amide / tetrahydrofuran
2: sodium tetrahydroborate / methanol
3: dibromotriphenylphosphorane / acetonitrile
4: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate / water; 1,4-dioxane
5: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0); potassium acetate; sodium carbonate; lithium diisopropyl amide; dibromotriphenylphosphorane;
In
tetrahydrofuran; 1,4-dioxane; methanol; water; toluene; acetonitrile;
4: |Miyaura Borylation Reaction;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: magnesium / diethyl ether
2: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / water
3: boron tribromide / dichloromethane / -80 °C
4: pyridine
5: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / water; toluene
With
pyridine; tetrakis(triphenylphosphine) palladium(0); boron tribromide; sodium carbonate; potassium carbonate; magnesium;
In
diethyl ether; dichloromethane; water; toluene;
2: |Suzuki Coupling;