racemic 1-Ph-2-tBu-3-Me-1H-2,1-benzazaborole

Base Information

Chemical Name:racemic 1-Ph-2-tBu-3-Me-1H-2,1-benzazaborole
CAS No.:1613019-95-6
Molecular Formula:C₁₈H₂₂BN
Molecular Weight:263.19
Hs Code.:

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Chemical Property of racemic 1-Ph-2-tBu-3-Me-1H-2,1-benzazaborole

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Technology Process of racemic 1-Ph-2-tBu-3-Me-1H-2,1-benzazaborole

There total 3 articles about racemic 1-Ph-2-tBu-3-Me-1H-2,1-benzazaborole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1436410-11-5
C₁₇H₁₉BClN

: 917-54-4
methyllithium

: 1613019-95-6
racemic 1-Ph-2-tBu-3-Me-1H-2,1-benzazaborole

Guidance literature:: In diethyl ether; toluene; at 0 - 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1039/c4dt01445f

Reference yield:

: [2-(CH=NtBu)C₆H₄]BPhCl

: 1613019-95-6
racemic 1-Ph-2-tBu-3-Me-1H-2,1-benzazaborole

Guidance literature:: Multi-step reaction with 3 steps

1: potassium mirror / toluene / 72 h / 20 °C

2: 2 h / 20 °C

3: tetrahydrofuran / 0.5 h

With potassium mirror; In tetrahydrofuran; toluene;
DOI:10.1039/c4dt00812j

Reference yield:

: C₃₄H₃₈B₂N₂

: 1613019-95-6
racemic 1-Ph-2-tBu-3-Me-1H-2,1-benzazaborole

Guidance literature:: Multi-step reaction with 2 steps

1: 2 h / 20 °C

2: tetrahydrofuran / 0.5 h

In tetrahydrofuran;
DOI:10.1039/c4dt00812j