4,6-O-benzylidene-2<(N-Z)-amino>-2-deoxy-D-gluconic acid azide

Base Information

Chemical Name:4,6-O-benzylidene-2<(N-Z)-amino>-2-deoxy-D-gluconic acid azide
CAS No.:79943-46-7
Molecular Formula:C₂₃H₂₅N₅O₈
Molecular Weight:499.48
Hs Code.:

Synonyms:

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Chemical Property of 4,6-O-benzylidene-2<(N-Z)-amino>-2-deoxy-D-gluconic acid azide

Chemical Property:

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Technology Process of 4,6-O-benzylidene-2<(N-Z)-amino>-2-deoxy-D-gluconic acid azide

There total 8 articles about 4,6-O-benzylidene-2<(N-Z)-amino>-2-deoxy-D-gluconic acid azide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 79943-45-6
4,6-O-benzylidene-2<(N-Z)-amino>-2-deoxy-D-gluconic acid hydrazide

: 79943-46-7
4,6-O-benzylidene-2<(N-Z)-amino>-2-deoxy-D-gluconic acid azide

Guidance literature:: With hydrogenchloride; sodium nitrite; In N,N-dimethyl-formamide; at -15 - -10 ℃;

Reference yield:

: 3646-68-2
D-glucosaminic acid

: 79943-46-7
4,6-O-benzylidene-2<(N-Z)-amino>-2-deoxy-D-gluconic acid azide

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / HCl / 16 h / Ambient temperature

2: 73 percent / 6 N HCl/NaNO₂, triethylamine / dimethylformamide / 17 h / -10 °C

3: 60 percent / 98percent N₂H₄

4: 6 N HCl/NaNO₂ / dimethylformamide / -15 - -10 °C

With hydrogenchloride; hydrazine hydrate; triethylamine; sodium nitrite; In N,N-dimethyl-formamide;

Reference yield:

: 40149-90-4
4,6-O-benzylideneglucosaminic acid ethyl ester hydrochloride

: 79943-46-7
4,6-O-benzylidene-2<(N-Z)-amino>-2-deoxy-D-gluconic acid azide

Guidance literature:: Multi-step reaction with 3 steps

1: 73 percent / 6 N HCl/NaNO₂, triethylamine / dimethylformamide / 17 h / -10 °C

2: 60 percent / 98percent N₂H₄

3: 6 N HCl/NaNO₂ / dimethylformamide / -15 - -10 °C

With hydrogenchloride; hydrazine hydrate; triethylamine; sodium nitrite; In N,N-dimethyl-formamide;