Butyric acid 4-[(3aS,3bS,6aR,6bR)-6b-(4-butyryloxy-phenyl)-3,6-dicyclohexylidene-2,5-dioxo-hexahydro-1,4-dioxa-cyclobutadicyclopenten-3b-yl]-phenyl ester

Base Information

Chemical Name:Butyric acid 4-[(3aS,3bS,6aR,6bR)-6b-(4-butyryloxy-phenyl)-3,6-dicyclohexylidene-2,5-dioxo-hexahydro-1,4-dioxa-cyclobutadicyclopenten-3b-yl]-phenyl ester
CAS No.:137174-71-1
Molecular Formula:C₄₀H₄₄O₈
Molecular Weight:652.785
Hs Code.:

Butyric acid 4-[(3aS,3bS,6aR,6bR)-6b-(4-butyryloxy-phenyl)-3,6-dicyclohexylidene-2,5-dioxo-hexahydro-1,4-dioxa-cyclobutadicyclopenten-3b-yl]-phenyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Butyric acid 4-[(3aS,3bS,6aR,6bR)-6b-(4-butyryloxy-phenyl)-3,6-dicyclohexylidene-2,5-dioxo-hexahydro-1,4-dioxa-cyclobutadicyclopenten-3b-yl]-phenyl ester

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Technology Process of Butyric acid 4-[(3aS,3bS,6aR,6bR)-6b-(4-butyryloxy-phenyl)-3,6-dicyclohexylidene-2,5-dioxo-hexahydro-1,4-dioxa-cyclobutadicyclopenten-3b-yl]-phenyl ester

There total 3 articles about Butyric acid 4-[(3aS,3bS,6aR,6bR)-6b-(4-butyryloxy-phenyl)-3,6-dicyclohexylidene-2,5-dioxo-hexahydro-1,4-dioxa-cyclobutadicyclopenten-3b-yl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 16.6%

: 137174-69-7
Butyric acid 4-(4-cyclohexylidene-5-oxo-4,5-dihydro-furan-2-yl)-phenyl ester

: 137174-71-1
Butyric acid 4-[(3aS,3bS,6aR,6bR)-6b-(4-butyryloxy-phenyl)-3,6-dicyclohexylidene-2,5-dioxo-hexahydro-1,4-dioxa-cyclobutadicyclopenten-3b-yl]-phenyl ester

: 137202-52-9
C₄₀H₄₄O₈

Guidance literature:: Irradiation;

Reference yield:

: 959251-52-6
3-Cyclohexylidene-5-(4-hydroxy-phenyl)-3H-furan-2-one

: 137174-71-1
Butyric acid 4-[(3aS,3bS,6aR,6bR)-6b-(4-butyryloxy-phenyl)-3,6-dicyclohexylidene-2,5-dioxo-hexahydro-1,4-dioxa-cyclobutadicyclopenten-3b-yl]-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂

2: 20.4 percent / Irradiation

With triethylamine; In dichloromethane;

Reference yield:

: 959251-49-1
Acetic acid 4-(4-cyclohexylidene-5-oxo-4,5-dihydro-furan-2-yl)-phenyl ester

: 137174-71-1
Butyric acid 4-[(3aS,3bS,6aR,6bR)-6b-(4-butyryloxy-phenyl)-3,6-dicyclohexylidene-2,5-dioxo-hexahydro-1,4-dioxa-cyclobutadicyclopenten-3b-yl]-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Al(OiPr)3 / CH₂Cl₂; methanol / 2 h / Heating

2: triethylamine / CH₂Cl₂

3: 20.4 percent / Irradiation

With aluminum isopropoxide; triethylamine; In methanol; dichloromethane;