Technology Process of Benzenesulfonyl-9 dodecane diol-1,10 diacetate
There total 2 articles about Benzenesulfonyl-9 dodecane diol-1,10 diacetate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 74 percent / NaI / dimethylformamide / 42 h / 65 °C
With
sodium iodide;
In
N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(86)80010-2
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 74 percent / NaI / dimethylformamide / 42 h / 65 °C
With
sodium iodide;
In
N,N-dimethyl-formamide;
DOI:10.1016/0040-4020(86)80010-2
- Guidance literature:
-
Multi-step reaction with 3 steps
1: powdered sodium hydroxide / dioxane / 2 h / Ambient temperature; further solvents were also used
2: Adogen, sodium dithionite, NaHCO3 / cyclohexane; H2O / 2 h / Heating
3: pyridine / 4 h / Ambient temperature
With
sodium hydroxide; sodium dithionite; triisooctyl amine; sodium hydrogencarbonate;
In
1,4-dioxane; pyridine; cyclohexane; water;
DOI:10.1016/0040-4020(86)80010-2
