C₃₉H₅₂O₄

Base Information

Chemical Name:C₃₉H₅₂O₄
CAS No.:127718-22-3
Molecular Formula:C₃₉H₅₂O₄
Molecular Weight:584.839
Hs Code.:

C<sub>39</sub>H<sub>52</sub>O<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₉H₅₂O₄

Chemical Property:

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Technology Process of C₃₉H₅₂O₄

There total 16 articles about C₃₉H₅₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 106-25-2
Nerol

: 127718-22-3
C₃₉H₅₂O₄

Guidance literature:: Multi-step reaction with 11 steps

1: Sharpless oxidation

3: 60 percent / imidazole / dimethylformamide / Ambient temperature

4: LDA / tetrahydrofuran / -40 °C

5: 91 percent / LiAlH₄ / tetrahydrofuran / 1.5 h / -50 °C

6: pyridine / 36 h / Ambient temperature

7: Pr₂NEt / 24 h / Ambient temperature

8: n-Bu₄NF / tetrahydrofuran / 3.5 h / 0 °C

9: n-Bu₃P / pyridine / 24 h / Ambient temperature

10: 99.7 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 14 h / -20 - -10 °C

With 1H-imidazole; lithium aluminium tetrahydride; dipropylethylamine; tributylphosphine; tetrabutyl ammonium fluoride; 3-chloro-benzenecarboperoxoic acid; lithium diisopropyl amide; In tetrahydrofuran; pyridine; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(01)80742-5

Reference yield:

: 127760-69-4
(2E, 4R)-2,4-dimethyl-2-hexen-1-ol

: 127718-22-3
C₃₉H₅₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: PCC / CH₂Cl₂ / 0.5 h / 0 - 25 °C

With pyridinium chlorochromate; In dichloromethane;
DOI:10.1016/S0040-4039(01)80742-5

Reference yield:

: 76-83-5
trityl chloride

: 127718-22-3
C₃₉H₅₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / 36 h / Ambient temperature

2: Pr₂NEt / 24 h / Ambient temperature

3: n-Bu₄NF / tetrahydrofuran / 3.5 h / 0 °C

4: n-Bu₃P / pyridine / 24 h / Ambient temperature

5: 99.7 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 14 h / -20 - -10 °C

With dipropylethylamine; tributylphosphine; tetrabutyl ammonium fluoride; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; pyridine; dichloromethane;
DOI:10.1016/S0040-4039(01)80742-5