{(CO)4Fe}Cl{((CH₃)2CH)2C₆H₃O}PCH₂Cl

Base Information

Chemical Name:{(CO)4Fe}Cl{((CH₃)2CH)2C₆H₃O}PCH₂Cl
CAS No.:154155-87-0
Molecular Formula:C₁₇H₁₉Cl₂FeO₅P
Molecular Weight:461.062
Hs Code.:

{(CO)4Fe}Cl{((CH<sub>3</sub>)2CH)2C<sub>6</sub>H<sub>3</sub>O}PCH<sub>2</sub>Cl

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Chemical Property of {(CO)4Fe}Cl{((CH₃)2CH)2C₆H₃O}PCH₂Cl

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Technology Process of {(CO)4Fe}Cl{((CH₃)2CH)2C₆H₃O}PCH₂Cl

There total 1 articles about {(CO)4Fe}Cl{((CH₃)2CH)2C₆H₃O}PCH₂Cl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 15321-51-4
diiron nonacarbonyl

: 154019-19-9
{((CH₃)2CH)2C₆H₃}OPClCH₂Cl

: 154155-87-0
{(CO)4Fe}Cl{((CH₃)2CH)2C₆H₃O}PCH₂Cl

Guidance literature:: In petroleum ether; byproducts: Fe(CO)5; under exclusion of air; addn. equimolar amt. P-compd. to suspn. Fe2(CO)9 in petroleum ether (40/60), stirred (20°C, 12-16 h); evapn. volatile compds. (20°C, 0.1 mbar), short column distn. of residue (0.01 mbar), elem. anal.;
DOI:10.1016/0022-328X(93)83348-Y

Reference yield: 44.0%

: 15321-51-4
diiron nonacarbonyl

: 154155-87-0
{(CO)4Fe}Cl{((CH₃)2CH)2C₆H₃O}PCH₂Cl

: (CO)10Fe₃{((CH₃)2CH)2C₆H₃OPCH₂}

Guidance literature:: In petroleum ether; byproducts: Fe(CO)5, FeCl2, CO; under exclusion of air; addn. excess Fe2(CO)9 to soln. P-complex in petroleum ether (40/60), mixt. heated (60°C, 1 h); evapn. (20°C, 0.1 mbar), residue extd. (CH2Cl2, twice), extracts concd., column chromy. (silica gel Si 60, petroleum ether (40/60)), evapn., elem. anal.;
DOI:10.1016/0022-328X(93)83348-Y