(η2-O,P-2-PPh2-4-Me-6-tBu-C6H3O)2AlMe

Base Information

Chemical Name:(η2-O,P-2-PPh2-4-Me-6-tBu-C6H3O)2AlMe
CAS No.:1172124-03-6
Molecular Formula:C₄₇H₅₁AlO₂P₂
Molecular Weight:736.85
Hs Code.:

Synonyms:

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Chemical Property of (η2-O,P-2-PPh2-4-Me-6-tBu-C6H3O)2AlMe

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Technology Process of (η2-O,P-2-PPh2-4-Me-6-tBu-C6H3O)2AlMe

There total 1 articles about (η2-O,P-2-PPh2-4-Me-6-tBu-C6H3O)2AlMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 75-24-1
trimethylaluminum

: 207291-28-9
2-(diphenylphosphanyl)-4-methyl-6-tert-butylphenol

: 1172124-03-6
(η2-O,P-2-PPh2-4-Me-6-tBu-C6H3O)2AlMe

Guidance literature:: In toluene; byproducts: CH4; (N2); addn. of soln. of 2 equiv. of phenol deriv. in toluene to toluene soln. of 1 equiv. of aluminium compd. at -35°C, warming to room temp., stirring for 2 h; evapn., addn. of pentane, filtration, drying in vac., elem. anal.;
DOI:10.1021/om9003362

Reference yield: 60.0%

: 109-99-9,24979-97-3,77392-70-2
tetrahydrofuran

: 1172124-03-6
(η2-O,P-2-PPh2-4-Me-6-tBu-C6H3O)2AlMe

: 1109-15-5
tris(pentafluorophenyl)borate

: 1172124-09-2
[(2-PPh₂-4-Me-6-tBu-C₆H₃O)2Al][MeB(C₆F₅)3]

Guidance literature:: In dichloromethane; (N2); dissolving 1:1 mixt. of boron compd. and aluminium compd. in CH2Cl2, stirring at room temp. for 1 h; evapn., addn. of cold pentane, isolation of solid, drying in vac., elem.anal.;
DOI:10.1021/om9003362

Reference yield:

: 1172124-03-6
(η2-O,P-2-PPh2-4-Me-6-tBu-C6H3O)2AlMe

: (η2-O,P-2-PPh2-4-Me-6-tBu-C6H3O)3Al

Guidance literature:: With CH₃CH₂CH₂CH₂OH or (CH₃)2CHOH; In not given; (N2); treatment of aluminium compd. with 1 equiv. of alcohol deriv.;
DOI:10.1021/om9003362