1,1'-di(cyanomethyl)ferrocene

Base Information

• Chemical Name: 1,1'-di(cyanomethyl)ferrocene
• CAS No.: 32677-74-0
• Molecular Formula: C₁₄H₁₂FeN₂
• Molecular Weight: 264.11

Synonyms:

Chemical Property of 1,1'-di(cyanomethyl)ferrocene

Chemical Property:

Purity/Quality:

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Technology Process of 1,1'-di(cyanomethyl)ferrocene

There total 3 articles about 1,1'-di(cyanomethyl)ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

1,1'-dihydroxymethylferrocene → 1,1'-di(cyanomethyl)ferrocene (32677-74-0)

Guidance literature:

With potassium cyanide; phosphorus trichloride; In tetrahydrofuran; water; Fe-complex in THF was reacted with PCl3 at 25°C for 2 h under N2, then reacted with KCN in H2O for 1 h;

DOI:10.1021/ja00325a027

Reference yield: 52.0%

potassium cyanide + 1,1'-dihydroxymethylferrocene → 1,1'-di(cyanomethyl)ferrocene (32677-74-0)

Guidance literature:

With pyridine; phosphorus trichloride; In tetrahydrofuran; react. with PCl3-pyridine, then with KCN-H2O;

DOI:10.1039/a904278d

Reference yield: 49.0%

potassium cyanide + 1,1'-bis(chloromethyl)ferrocene → 1,1'-di(cyanomethyl)ferrocene (32677-74-0)

Guidance literature:

In tetrahydrofuran; water; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique; Cooling with ice; Enzymatic reaction;

DOI:10.1016/j.jorganchem.2013.05.006

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