Methyl (3,4-di-O-benzyl-2-acetimido-2-deoxy-β-D-glucopyranosyl)(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,6-di-O-benzyl-α-D-mannopyranoside-4,6''-methylidene acetal

Base Information

Chemical Name:Methyl (3,4-di-O-benzyl-2-acetimido-2-deoxy-β-D-glucopyranosyl)(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,6-di-O-benzyl-α-D-mannopyranoside-4,6''-methylidene acetal
CAS No.:245365-59-7
Molecular Formula:C₇₁H₇₉NO₁₆
Molecular Weight:1202.41
Hs Code.:

Methyl (3,4-di-O-benzyl-2-acetimido-2-deoxy-β-D-glucopyranosyl)(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,6-di-O-benzyl-α-D-mannopyranoside-4,6''-methylidene acetal

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Chemical Property of Methyl (3,4-di-O-benzyl-2-acetimido-2-deoxy-β-D-glucopyranosyl)(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,6-di-O-benzyl-α-D-mannopyranoside-4,6''-methylidene acetal

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Technology Process of Methyl (3,4-di-O-benzyl-2-acetimido-2-deoxy-β-D-glucopyranosyl)(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,6-di-O-benzyl-α-D-mannopyranoside-4,6''-methylidene acetal

There total 2 articles about Methyl (3,4-di-O-benzyl-2-acetimido-2-deoxy-β-D-glucopyranosyl)(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,6-di-O-benzyl-α-D-mannopyranoside-4,6''-methylidene acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 245365-58-6
Methyl (3,4-di-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,6-di-O-benzyl-α-D-mannopyranoside-4,6''-methylidene acetal

: 245365-59-7
Methyl (3,4-di-O-benzyl-2-acetimido-2-deoxy-β-D-glucopyranosyl)(1->2)-(3,4,6-tri-O-benzyl-α-D-mannopyranosyl)-(1->3)-2,6-di-O-benzyl-α-D-mannopyranoside-4,6''-methylidene acetal

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine monohydrate / ethanol / 18 h / Heating

2: pyridine / 4 h / 20 °C

With pyridine; hydrazine hydrate; In ethanol; 1: Hydrolysis / 2: Acetylation;
DOI:10.1002/(SICI)1521-3765(19990802)5:8<2281::AID-CHEM2281>3.0.CO;2-D