Technology Process of C25H23N3O7
There total 12 articles about C25H23N3O7 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: pyridine / dichloromethane; water
2: thionyl chloride
3: pyridine
4: sodium methylate; water / tetrahydrofuran; methanol
5: phosphorus tribromide / tetrahydrofuran
6: Reflux
7: potassium tert-butylate / tetrahydrofuran
8: sodium hydroxide; water / tetrahydrofuran
With
pyridine; thionyl chloride; potassium tert-butylate; water; sodium methylate; phosphorus tribromide; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water;
7: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.bmcl.2012.11.018
- Guidance literature:
-
Multi-step reaction with 7 steps
1: thionyl chloride
2: pyridine
3: sodium methylate; water / tetrahydrofuran; methanol
4: phosphorus tribromide / tetrahydrofuran
5: Reflux
6: potassium tert-butylate / tetrahydrofuran
7: sodium hydroxide; water / tetrahydrofuran
With
pyridine; thionyl chloride; potassium tert-butylate; water; sodium methylate; phosphorus tribromide; sodium hydroxide;
In
tetrahydrofuran; methanol;
6: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.bmcl.2012.11.018
- Guidance literature:
-
Multi-step reaction with 12 steps
1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran
2: potassium hydroxide; water / methanol / Reflux
3: borane-THF
4: sodium hydroxide; water / tetrahydrofuran
5: pyridine / dichloromethane; water
6: thionyl chloride
7: pyridine
8: sodium methylate; water / tetrahydrofuran; methanol
9: phosphorus tribromide / tetrahydrofuran
10: Reflux
11: potassium tert-butylate / tetrahydrofuran
12: sodium hydroxide; water / tetrahydrofuran
With
pyridine; thionyl chloride; borane-THF; di-isopropyl azodicarboxylate; potassium tert-butylate; water; sodium methylate; phosphorus tribromide; triphenylphosphine; potassium hydroxide; sodium hydroxide;
In
tetrahydrofuran; methanol; dichloromethane; water;
1: |Mitsunobu Displacement / 11: |Horner-Wadsworth-Emmons Olefination;
DOI:10.1016/j.bmcl.2012.11.018