(PPh3)2Pt(η3-CH2C(N(i-Pr)2)CHPh)TOf

Base Information

Chemical Name:(PPh3)2Pt(η3-CH2C(N(i-Pr)2)CHPh)TOf
CAS No.:539847-99-9
Molecular Formula:C₇H₇O₃S*C₅₁H₅₂NP₂Pt
Molecular Weight:1107.2
Hs Code.:

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Chemical Property of (PPh3)2Pt(η3-CH2C(N(i-Pr)2)CHPh)TOf

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Technology Process of (PPh3)2Pt(η3-CH2C(N(i-Pr)2)CHPh)TOf

There total 2 articles about (PPh3)2Pt(η3-CH2C(N(i-Pr)2)CHPh)TOf which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 12120-15-9
ethylenebis(triphenylphosphine)platinum⁽⁰⁾

: 21541-60-6
3-phenylprop-2-ynyl 4-methylbenzenesulfonate

: 108-18-9
diisopropylamine

: 539847-99-9
(PPh3)2Pt(η3-CH2C(N(i-Pr)2)CHPh)TOf

Guidance literature:: In dichloromethane; ligand was added to stirred soln. of Pt-complex in CH2Cl2 at 0°C,warmed to room temp., amine was introduced, stirred for 30 min under Ar; volatiles were removed under reduced pressure, washed with hexane, driedunder vac. for several d;
DOI:10.1016/S0020-1693(02)01168-4

Reference yield:

: 173539-25-8
[(PPh3)2Pt(η(3)-CH2CCPh)]OSO2C6H4CH3

: 626-23-3
Di-sec-butylamin

: 108-18-9
diisopropylamine

: 539847-99-9
(PPh3)2Pt(η3-CH2C(N(i-Pr)2)CHPh)TOf

: 539848-02-7
(PPh3)2Pt(η3-CH2C(N(sec-Bu)2)CHPh)TOf

Guidance literature:: In dichloromethane; stirred mixt. of amines in CH2Cl2 was added to Pt-complex in CH2Cl2, 15 min under Ar; volatiles were removed under reduced pressure, dried for several h, not sepd.;
DOI:10.1016/S0020-1693(02)01168-4