thymidine 5'-(6-deoxy-α-D-glucopyranosyl diphosphate)

Base Information

Chemical Name:thymidine 5'-(6-deoxy-α-D-glucopyranosyl diphosphate)
CAS No.:24988-24-7
Molecular Formula:C₁₆H₂₆N₂O₁₅P₂
Molecular Weight:548.334
Hs Code.:

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Chemical Property of thymidine 5'-(6-deoxy-α-D-glucopyranosyl diphosphate)

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Technology Process of thymidine 5'-(6-deoxy-α-D-glucopyranosyl diphosphate)

There total 15 articles about thymidine 5'-(6-deoxy-α-D-glucopyranosyl diphosphate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2147-59-3,16268-29-4,24960-12-1,24988-24-7,26467-14-1,27180-11-6,51897-79-1,62012-79-7
thymidine diphosphate-L-rhamnose

Guidance literature:: Aus Kulturen v. Lactobacillus acidophilus R-26;
DOI:10.1016/0006-3002(60)91602-4

Reference yield:

: 488-79-9
6-deoxy-D-glucose

: 24988-24-7,62012-79-7
thymidine 5'-(6-deoxy-α-D-glucopyranosyl diphosphate)

Guidance literature:: Multi-step reaction with 7 steps

1.1: 2.8 g / pyridine / 20 °C

2.1: 81.5 percent / zinc iodide / CH₂Cl₂ / 2 h / Heating

3.1: NaOMe / methanol; toluene / 2 h / 20 °C

4.1: NaH / dimethylformamide / 2 h / 20 °C

4.2: 480 mg / dimethylformamide

5.1: 76 percent / trifluoromethanesulfonic acid; N-iodosuccinamide / CH₂Cl₂ / 0.5 h / -30 °C

6.1: H₂; NaHCO₃ / Pd/C / methanol / 20 °C

7.1: Mg⁽²⁺⁾; NTP; E_.p / thymidylyl-transferase / 0.5 h / 37 °C

With pyridine; N-Iodosuccinamide; trifluorormethanesulfonic acid; magnesium(II); hydrogen; sodium methylate; sodium hydride; sodium hydrogencarbonate; zinc(II) iodide; palladium on activated charcoal; thymidylyl-transferase; In methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja001444y

Reference yield:

: 97-30-3
methyl-alpha-D-glucopyranoside

: 24988-24-7,62012-79-7
thymidine 5'-(6-deoxy-α-D-glucopyranosyl diphosphate)

Guidance literature:: Multi-step reaction with 11 steps

1.1: CCl₄; Ph₃P

2.1: pyridine

3.1: LiAlH₄ / tetrahydrofuran / 10 h / Heating

4.1: HCl; AcOH / 10 h / 95 °C

5.1: 2.8 g / pyridine / 20 °C

6.1: 81.5 percent / zinc iodide / CH₂Cl₂ / 2 h / Heating

7.1: NaOMe / methanol; toluene / 2 h / 20 °C

8.1: NaH / dimethylformamide / 2 h / 20 °C

8.2: 480 mg / dimethylformamide

9.1: 76 percent / trifluoromethanesulfonic acid; N-iodosuccinamide / CH₂Cl₂ / 0.5 h / -30 °C

10.1: H₂; NaHCO₃ / Pd/C / methanol / 20 °C

11.1: Mg⁽²⁺⁾; NTP; E_.p / thymidylyl-transferase / 0.5 h / 37 °C

With pyridine; hydrogenchloride; tetrachloromethane; lithium aluminium tetrahydride; N-Iodosuccinamide; trifluorormethanesulfonic acid; magnesium(II); hydrogen; sodium methylate; sodium hydride; sodium hydrogencarbonate; acetic acid; triphenylphosphine; zinc(II) iodide; palladium on activated charcoal; thymidylyl-transferase; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ja001444y