7-Methoxy-1-phenyl-3-oxo-1,2,3,9a-tetrahydrofluorene

Base Information

Chemical Name:7-Methoxy-1-phenyl-3-oxo-1,2,3,9a-tetrahydrofluorene
CAS No.:75258-89-8
Molecular Formula:C₂₀H₁₈O₂
Molecular Weight:290.362
Hs Code.:

Synonyms:

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Chemical Property of 7-Methoxy-1-phenyl-3-oxo-1,2,3,9a-tetrahydrofluorene

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Technology Process of 7-Methoxy-1-phenyl-3-oxo-1,2,3,9a-tetrahydrofluorene

There total 4 articles about 7-Methoxy-1-phenyl-3-oxo-1,2,3,9a-tetrahydrofluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 75258-88-7
1,2-trans-2-Carbomethoxy-7-methoxy-3-oxo-1-phenyl-1,2,3,9a-tetrahydrofluorene

: 75258-89-8
7-Methoxy-1-phenyl-3-oxo-1,2,3,9a-tetrahydrofluorene

Guidance literature:: With sulfuric acid; In water; acetic acid; for 0.75h; Heating;

Reference yield:

: 5111-70-6
5-methoxy-1-indanone

: 75258-89-8
7-Methoxy-1-phenyl-3-oxo-1,2,3,9a-tetrahydrofluorene

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / 4percent KOH / ethanol / 1 h / Ambient temperature

2: 75 percent / NaH / methanol / 1) reflux, 3 h 2) room temperature

3: 69 percent / conc. H₂SO₄ / acetic acid; H₂O / 0.75 h / Heating

With potassium hydroxide; sulfuric acid; sodium hydride; In methanol; ethanol; water; acetic acid;

Reference yield:

: 5111-69-3
5-methoxyindane

: 75258-89-8
7-Methoxy-1-phenyl-3-oxo-1,2,3,9a-tetrahydrofluorene

Guidance literature:: Multi-step reaction with 4 steps

1: 68 percent / CrO₃ / acetic acid; propionic acid; H₂O / 1) 5 - 10 deg C, 1 h 2) room temperature

2: 88 percent / 4percent KOH / ethanol / 1 h / Ambient temperature

3: 75 percent / NaH / methanol / 1) reflux, 3 h 2) room temperature

4: 69 percent / conc. H₂SO₄ / acetic acid; H₂O / 0.75 h / Heating

With chromium(VI) oxide; potassium hydroxide; sulfuric acid; sodium hydride; In methanol; ethanol; water; acetic acid; propionic acid;