3,4,5,6-Tetramethoxy-1-methoxymethyloxy-2-oxiranylbenzene

Base Information

Chemical Name:3,4,5,6-Tetramethoxy-1-methoxymethyloxy-2-oxiranylbenzene
CAS No.:104202-47-3
Molecular Formula:C₁₄H₂₀O₇
Molecular Weight:300.309
Hs Code.:

Synonyms:

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Chemical Property of 3,4,5,6-Tetramethoxy-1-methoxymethyloxy-2-oxiranylbenzene

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Technology Process of 3,4,5,6-Tetramethoxy-1-methoxymethyloxy-2-oxiranylbenzene

There total 5 articles about 3,4,5,6-Tetramethoxy-1-methoxymethyloxy-2-oxiranylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 3086-29-1
trimethylsulfonium chloride

: 104202-51-9
2-Methoxymethyloxy-3,4,5,6-tetramethoxybenzaldehyde

: 104202-47-3
3,4,5,6-Tetramethoxy-1-methoxymethyloxy-2-oxiranylbenzene

Guidance literature:: With sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride; In tetrahydrofuran; Ambient temperature;

Reference yield:

: 21450-56-6
1,2,3,4-tetramethoxybenzene

: 104202-47-3
3,4,5,6-Tetramethoxy-1-methoxymethyloxy-2-oxiranylbenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 90 percent / POCl₃

2: 1.) bis(2,4-dinitrophenyl)diselenide, 80percent H₂O₂, 2.) KOH / 1.) CH₂Cl₂, H₂O, 3 h, 2.) MeOH, 1 h

3: 97 percent / NaOH, TEBA / tetrahydrofuran / 4 h

4: 1.) 1.6 M BuLi / 1.) hexane, THF, 3 h, - 5 deg C, 2.) 1 h

5: 53 percent / NaOH, TEBA / tetrahydrofuran / Ambient temperature

With potassium hydroxide; sodium hydroxide; n-butyllithium; bis(2,4-dinitrophenyl) diselenide; N-benzyl-N,N,N-triethylammonium chloride; dihydrogen peroxide; trichlorophosphate; In tetrahydrofuran;

Reference yield:

: 30225-99-1
2,3,4,5-Tetramethoxyphenol

: 104202-47-3
3,4,5,6-Tetramethoxy-1-methoxymethyloxy-2-oxiranylbenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / NaOH, TEBA / tetrahydrofuran / 4 h

2: 1.) 1.6 M BuLi / 1.) hexane, THF, 3 h, - 5 deg C, 2.) 1 h

3: 53 percent / NaOH, TEBA / tetrahydrofuran / Ambient temperature

With sodium hydroxide; n-butyllithium; N-benzyl-N,N,N-triethylammonium chloride; In tetrahydrofuran;