C₁₄H₁₂N₄OS₂

Base Information

• Chemical Name: C₁₄H₁₂N₄OS₂
• CAS No.: 1255517-72-6
• Molecular Formula: C₁₄H₁₂N₄OS₂
• Molecular Weight: 316.407
• Mol file: 1255517-72-6.mol

Synonyms:

Chemical Property of C₁₄H₁₂N₄OS₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₁₂N₄OS₂

There total 4 articles about C₁₄H₁₂N₄OS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3-ethylrhodanin (7648-01-3) + C9H7Cl2N3 (1255517-58-8) → C14H12N4OS2 (1255517-72-6)

Guidance literature:

With piperidine; acetic acid; In ethanol; for 72h; Reflux;

DOI:10.1134/S1070363210080219

Reference yield:

N-trichlorovinyl-benzimidoyl chloride (54735-74-9) → C14H12N4OS2 (1255517-72-6)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine hydrate / tetrahydrofuran / 12 h / 20 - 25 °C

2: piperidine; acetic acid / ethanol / 72 h / Reflux

With piperidine; hydrazine hydrate; acetic acid; In tetrahydrofuran; ethanol;

DOI:10.1134/S1070363210080219

Reference yield:

C9H9Cl2N3 (1255517-56-6) → C14H12N4OS2 (1255517-72-6)

Guidance literature:

Multi-step reaction with 2 steps

1: manganese(IV) oxide / 1,4-dioxane / 2 h / Reflux

2: piperidine; acetic acid / ethanol / 72 h / Reflux

With piperidine; manganese(IV) oxide; acetic acid; In 1,4-dioxane; ethanol;

DOI:10.1134/S1070363210080219

upstream raw materials:

3-ethylrhodanin

C₉H₇Cl₂N₃

C₉H₉Cl₂N₃

N-trichlorovinyl-benzimidoyl chloride