N-(p-Methoxy-benzyloxycarbonyl)-L-glutamyl-γ--L-valin

Base Information

Chemical Name:N-(p-Methoxy-benzyloxycarbonyl)-L-glutamyl-γ--L-valin
CAS No.:13288-58-9
Molecular Formula:C₃₇H₄₇N₃O₁₁
Molecular Weight:709.794
Hs Code.:

N-(p-Methoxy-benzyloxycarbonyl)-L-glutamyl-γ-<bis-(2,4-dimethoxy-benzyl)-amid>-L-valin

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Chemical Property of N-(p-Methoxy-benzyloxycarbonyl)-L-glutamyl-γ--L-valin

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Technology Process of N-(p-Methoxy-benzyloxycarbonyl)-L-glutamyl-γ--L-valin

There total 5 articles about N-(p-Methoxy-benzyloxycarbonyl)-L-glutamyl-γ--L-valin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21209-48-3
p-methoxybenzyloxycarbonyl-Glu-OH

: 13288-58-9
N-(p-Methoxy-benzyloxycarbonyl)-L-glutamyl-γ--L-valin

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / dimethylformamide

2: (i) N-hydroxy-succinimide, DCC, CH₂Cl₂, (ii) /BRN= 2772692/

3: aq. NaOH / dioxane

4: (i) diethyl-prop-1-ynyl-amine, THF, (ii) /BRN= 1721775/, (iii) aq. NaOH, dioxane

With sodium hydroxide; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;
DOI:10.1002/cber.19681011038

Reference yield:

: 20781-23-1
bis(2,4-dimethoxybenzyl)amine

: 13288-58-9
N-(p-Methoxy-benzyloxycarbonyl)-L-glutamyl-γ--L-valin

Guidance literature:: Multi-step reaction with 3 steps

1: (i) N-hydroxy-succinimide, DCC, CH₂Cl₂, (ii) /BRN= 2772692/

2: aq. NaOH / dioxane

3: (i) diethyl-prop-1-ynyl-amine, THF, (ii) /BRN= 1721775/, (iii) aq. NaOH, dioxane

With sodium hydroxide; In 1,4-dioxane;
DOI:10.1002/cber.19681011038

Reference yield:

: 100232-93-7
p-methoxybenzyloxycarbonyl-Glu-α-OBzl

: 13288-58-9
N-(p-Methoxy-benzyloxycarbonyl)-L-glutamyl-γ--L-valin

Guidance literature:: Multi-step reaction with 3 steps

1: (i) N-hydroxy-succinimide, DCC, CH₂Cl₂, (ii) /BRN= 2772692/

2: aq. NaOH / dioxane

3: (i) diethyl-prop-1-ynyl-amine, THF, (ii) /BRN= 1721775/, (iii) aq. NaOH, dioxane

With sodium hydroxide; In 1,4-dioxane;
DOI:10.1002/cber.19681011038