C₅₁H₄₅BF₁₈N₂

Base Information

• Chemical Name: C₅₁H₄₅BF₁₈N₂
• CAS No.: 1421229-26-6
• Molecular Formula: C₅₁H₄₅BF₁₈N₂
• Molecular Weight: 1038.71
• Mol file: 1421229-26-6.mol

Synonyms:

Chemical Property of C₅₁H₄₅BF₁₈N₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₁H₄₅BF₁₈N₂

There total 2 articles about C₅₁H₄₅BF₁₈N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3,6-bis(trifluoromethyl)bromobenzene (328-70-1) → C51H45BF18N2 (1421229-26-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran / 4 h / 4 - 20 °C / Schlenk technique; Glovebox; Inert atmosphere

1.2: 2 h / -20 - 20 °C

2.1: toluene / 2 h / Schlenk technique; Glovebox; Inert atmosphere

With isopropylmagnesium chloride; In tetrahydrofuran; toluene;

DOI:10.1002/chem.201202840

Reference yield:

1,3-bis(trifluoromethyl)benzene (402-31-3) → C51H45BF18N2 (1421229-26-6)

Guidance literature:

Multi-step reaction with 3 steps

1.1: acetic acid; sulfuric acid; 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / water / 4 h / 5 - 45 °C

2.1: isopropylmagnesium chloride / tetrahydrofuran / 4 h / 4 - 20 °C / Schlenk technique; Glovebox; Inert atmosphere

2.2: 2 h / -20 - 20 °C

3.1: toluene / 2 h / Schlenk technique; Glovebox; Inert atmosphere

With 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione; sulfuric acid; isopropylmagnesium chloride; acetic acid; In tetrahydrofuran; water; toluene;

DOI:10.1002/chem.201202840

upstream raw materials:

3,6-bis(trifluoromethyl)bromobenzene

1,3-bis(trifluoromethyl)benzene