cis-2-Tosylbicyclo-<3.1.0>-hexan

Base Information

• Chemical Name: cis-2-Tosylbicyclo-<3.1.0>-hexan
• CAS No.: 98752-81-9
• Molecular Formula: C₁₃H₁₆O₂S
• Molecular Weight: 236.335
• Mol file: 98752-81-9.mol

Synonyms:

Chemical Property of cis-2-Tosylbicyclo-<3.1.0>-hexan

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cis-2-Tosylbicyclo-<3.1.0>-hexan

There total 4 articles about cis-2-Tosylbicyclo-<3.1.0>-hexan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

p-toluenesulfonyl chloride (98-59-9) → (1R,2R,5S)-2-(Toluene-4-sulfonyl)-bicyclo[3.1.0]hexane (37500-26-8,98752-81-9)

Guidance literature:

In dichloromethane; at 0 ℃; for 10.5h; Irradiation;

Reference yield:

1-tosylazocyclohexene (17344-06-8) → cis-2-Tosylbicyclo-<3.1.0>-hexan (37500-26-8,98752-81-9)

Guidance literature:

With acetic acid; In chloroform;

DOI:10.1021/jo00945a017

Reference yield:

p-toluenesulfonyl chloride (98-59-9) → (1R,2R,5S)-2-(Toluene-4-sulfonyl)-bicyclo[3.1.0]hexane (37500-26-8,98752-81-9) + cis-2-Tosylbicyclo-<3.1.0>-hexan (37500-26-8,98752-81-9)

Guidance literature:

In dichloromethane; at 0 ℃; for 25h; Yield given. Yields of byproduct given. Title compound not separated from byproducts; Irradiation;

upstream raw materials:

p-toluenesulfonyl chloride

1-tosylazocyclohexene