Welcome to LookChem.com Sign In|Join Free
  • or

Encyclopedia

Technology Process of trans-[Rh(CO)(pyridine)(PPh3)2]ClO4

trans-[Rh(CO)(pyridine)(PPh3)2]ClO4

Base Information
  • Chemical Name:trans-[Rh(CO)(pyridine)(PPh3)2]ClO4
  • CAS No.:34248-32-3
  • Molecular Formula:C42H35NOP2Rh*ClO4
  • Molecular Weight:834.05
  • Hs Code.:
trans-[Rh(CO)(pyridine)(PPh<sub>3</sub>)2]ClO<sub>4</sub>

Synonyms:

Suppliers and Price of trans-[Rh(CO)(pyridine)(PPh3)2]ClO4
Supply Marketing:
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
Total 0 raw suppliers
Chemical Property of trans-[Rh(CO)(pyridine)(PPh3)2]ClO4
Chemical Property:
Purity/Quality:
Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:
Useful:
Technology Process of trans-[Rh(CO)(pyridine)(PPh3)2]ClO4

There total 1 articles about trans-[Rh(CO)(pyridine)(PPh3)2]ClO4 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trans-[Rh(CO)(PPh<sub>3</sub>)2(OClO<sub>3</sub>)]
36593-52-9,32354-26-0

trans-[Rh(CO)(PPh3)2(OClO3)]

trans-[Rh(CO)(pyridine)(PPh<sub>3</sub>)2]ClO<sub>4</sub>
34248-32-3,55254-04-1

trans-[Rh(CO)(pyridine)(PPh3)2]ClO4

Guidance literature:
With pyridine; In dichloromethane; dichloromethane-d2; N2-atmosphere; addn. of 1 equiv. of pyridine to Rh-complex (in CH2Cl2:CD2Cl2=1:1); pptn. on addn. of light petroleum; elem. anal.;
DOI:10.1039/DT9940002875

Reference yield:

{Rh(CO)(P(C<sub>6</sub>H<sub>5</sub>)3)2(C<sub>5</sub>H<sub>5</sub>N)}<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup> = {Rh(CO)(P(C<sub>6</sub>H<sub>5</sub>)3)2(C<sub>5</sub>H<sub>5</sub>N)}ClO<sub>4</sub>
34248-32-3,55254-04-1

{Rh(CO)(P(C6H5)3)2(C5H5N)}(1+)*ClO4(1-) = {Rh(CO)(P(C6H5)3)2(C5H5N)}ClO4

sodium tetraphenyl borate
143-66-8

sodium tetraphenyl borate

{Rh(CO)(P(C<sub>6</sub>H<sub>5</sub>)3)(C<sub>5</sub>H<sub>5</sub>N)(S<sub>2</sub>CP(C<sub>6</sub>H<sub>5</sub>)3)}<sup>(1+)</sup>*B(C<sub>6</sub>H<sub>5</sub>)4<sup>(1-)</sup> = {Rh(CO)(P(C<sub>6</sub>H<sub>5</sub>)3)(C<sub>5</sub>H<sub>5</sub>N)(S<sub>2</sub>CP(C<sub>6</sub>H<sub>5</sub>)3)}B(C<sub>6</sub>H<sub>5</sub>)4

{Rh(CO)(P(C6H5)3)(C5H5N)(S2CP(C6H5)3)}(1+)*B(C6H5)4(1-) = {Rh(CO)(P(C6H5)3)(C5H5N)(S2CP(C6H5)3)}B(C6H5)4

Guidance literature:
With carbon disulfide; triphenylphosphine; In methanol; rhodium complex mixed with PPh3 (methanol); CS2 added; NaBPh4 added (methanol); cooled below 0°C for 30 min;; ppt. filtered; washed (cold methanol); dried in air; elem. anal.;;
upstream raw materials:

trans-[Rh(CO)(PPh3)2(OClO3)]

Post a RFQ

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

1 Customer Service

What can I do for you?
Get Best Price

Get Best Price for 34248-32-3

Total 8 Pictures about this product