1,3,4,6-Tetra-o-acetyl-2-amino-2-desoxy-D-glucopyranose hydrochloride

Base Information

• Chemical Name: 1,3,4,6-Tetra-o-acetyl-2-amino-2-desoxy-D-glucopyranose hydrochloride
• CAS No.: 1191127-63-5
• Molecular Formula: C₁₄H₂₁NO₉*ClH
• Molecular Weight: 383.783
• Mol file: 1191127-63-5.mol

Synonyms:

Chemical Property of 1,3,4,6-Tetra-o-acetyl-2-amino-2-desoxy-D-glucopyranose hydrochloride

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

1,3,4,6-Tetra-O-acetyl-2-amino-2-desoxy-D-glucopyranosehydrochloride 99% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,3,4,6-Tetra-o-acetyl-2-amino-2-desoxy-D-glucopyranose hydrochloride

There total 66 articles about 1,3,4,6-Tetra-o-acetyl-2-amino-2-desoxy-D-glucopyranose hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

1,3,4,6-tetra-O-acetyl-2-deoxy-2-(4-methoxybenzylidene)amino-β-D-glucopyranose (7597-81-1) → 1,3,4,6-tetra-O-acetyl-D-glucosamine hydrochloride (5432-46-2,10034-19-2,10034-20-5,34948-62-4,110253-00-4,1191127-63-5)

Guidance literature:

With hydrogenchloride; In acetone;

DOI:10.1021/jo9903499

Reference yield: 100.0%

1,3,4,6-tetra-O-acetyl-2-deoxy-2-{[(4-methoxyphenyl)methylidene]amino}-D-glucopyranose (114297-26-6) → 1,3,4,6-tetra-O-acetyl-D-glucosamine hydrochloride (5432-46-2,10034-19-2,10034-20-5,34948-62-4,110253-00-4,1191127-63-5)

Guidance literature:

With hydrogenchloride; In acetone;

DOI:10.1002/hlca.200590175

Reference yield: 97.0%

(2S,3R,4R,5S,6R)-6-(acetoxymethyl)-3-((E)-(4-methoxybenzylidene)amino)tetrahydro-2Hpyran-2,4,5-triyl triacetate (7597-81-1,34948-61-3,55628-19-8,74554-00-0,103382-86-1,114297-26-6) → 1,3,4,6-tetra-O-acetyl-D-glucosamine hydrochloride (5432-46-2,10034-19-2,10034-20-5,34948-62-4,110253-00-4,1191127-63-5)

Guidance literature:

With hydrogenchloride; In water; acetone; for 1.5h;

DOI:10.1016/j.bmc.2016.12.024

upstream raw materials:

(2S,3R,4R,5S,6R)-6-(acetoxymethyl)-3-((E)-(4-methoxybenzylidene)amino)tetrahydro-2Hpyran-2,4,5-triyl triacetate

1,3,4,6-tetra-O-acetyl-2-deoxy-2-(4-methoxybenzylidene)amino-β-D-glucopyranose

1,3,4,6-tetra-O-acetyl-2-deoxy-2-{[(4-methoxyphenyl)methylidene]amino}-D-glucopyranose

2--2-deoxy-D-glucopyranose

Downstream raw materials:

1,3,4,6-tetra-O-acetyl-2-amino-2-deoxy-alpha-D-glucopyranose

1,3,4,6-tetra-O-acetyl-2-deoxy-2-(2,2,2-trichloroacetamido)-β-D-glucopyranose

1,3,4,6-tetra-O-acetyl-2-deoxy-2-phthalimido-β-D-glucopyranose

1-acetoxy-3,4,6-tri-O-acetyl-2-deoxy-2-(4,5-dichlorophthalimido)-β-D-glucopyranoside

Refernces

• 1、 Mohammed, Aya A. M.,Okechukwu, Patrick N.,Shehadeh, Mayadah B.,Suaifan, Ghadeer A. R. Y.. "Design, synthesis and antimicrobial evaluation of novel glycosylated-fluoroquinolones derivatives". . . Retrieved 2020/07/04.
• 2、 -. "1,8-NAPHTHYRIDINE GLUCOSAMINE DERIVATIVES, THEIR USE IN THE TREATMENT OF MICROBIAL INFECTIONS, AND A METHOD FOR PREPARATION". Paragraph 049-050. . Retrieved 2020/06/10.