Technology Process of C71H75NO27
There total 20 articles about C71H75NO27 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: pyridine
3: 76 percent / BF3*OEt2, MS-AW300 / toluene; CH2Cl2 / -25 °C
4: CSA / methanol; CH2Cl2
5: 1) pyridine, 2) DMAP, pyridine / 1) 0 deg C, 2) 1,2-dichloroethane
6: PPh3 / benzene; H2O / 24 h / 50 °C
7: DMAP, pyridine
9: H2 / 10percent Pd-C / methanol
10: DMAP, pyridine
With
pyridine; dmap; MS-AW300; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; hydrogen; triphenylphosphine;
palladium on activated charcoal;
In
methanol; dichloromethane; water; toluene; benzene;
DOI:10.1016/S0040-4039(00)61790-2
- Guidance literature:
-
Multi-step reaction with 5 steps
1: PPh3 / benzene; H2O / 24 h / 50 °C
2: DMAP, pyridine
4: H2 / 10percent Pd-C / methanol
5: DMAP, pyridine
With
pyridine; dmap; hydrogen; triphenylphosphine;
palladium on activated charcoal;
In
methanol; water; benzene;
DOI:10.1016/S0040-4039(00)61790-2
- Guidance literature:
-
Multi-step reaction with 7 steps
1: CSA / methanol; CH2Cl2
2: 1) pyridine, 2) DMAP, pyridine / 1) 0 deg C, 2) 1,2-dichloroethane
3: PPh3 / benzene; H2O / 24 h / 50 °C
4: DMAP, pyridine
6: H2 / 10percent Pd-C / methanol
7: DMAP, pyridine
With
pyridine; dmap; camphor-10-sulfonic acid; hydrogen; triphenylphosphine;
palladium on activated charcoal;
In
methanol; dichloromethane; water; benzene;
DOI:10.1016/S0040-4039(00)61790-2