C₁₅H₁₆BrNO

Base Information

Chemical Name:C₁₅H₁₆BrNO
CAS No.:1629023-35-3
Molecular Formula:C₁₅H₁₆BrNO
Molecular Weight:306.202
Hs Code.:

Synonyms:

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Chemical Property of C₁₅H₁₆BrNO

Chemical Property:

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Technology Process of C₁₅H₁₆BrNO

There total 6 articles about C₁₅H₁₆BrNO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1435-51-4
1,3-dibromo-5-fluorobenzene

: 1629023-35-3
C₁₅H₁₆BrNO

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / 1-methyl-pyrrolidin-2-one / 24 h / 120 °C

2.1: lithium chloride / dimethyl sulfoxide; water / 3 h / 165 °C

3.1: tetrabutylammomium bromide; sodium hydroxide / toluene; water / 16 h / 20 °C

4.1: copper(l) cyanide; TurboGrignard / tetrahydrofuran / 1 h / 0 - 20 °C

5.1: ozone / dichloromethane; methanol / 1 h / -78 °C

5.2: 16 h / -78 - 20 °C

6.1: tetrahydrofuran / 16 h / -78 - 20 °C

With TurboGrignard; tetrabutylammomium bromide; copper(l) cyanide; sodium hydride; ozone; lithium chloride; sodium hydroxide; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; methanol; dichloromethane; water; dimethyl sulfoxide; toluene; 2.1: |Krapcho Dealkoxycarbonylation / 6.1: |Grignard Reaction;
DOI:10.1016/j.bmcl.2014.05.082

Reference yield:

: cyano-(3,5-dibromophenyl)acetic acid ethyl ester

: 1629023-35-3
C₁₅H₁₆BrNO

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium chloride / dimethyl sulfoxide; water / 3 h / 165 °C

2.1: tetrabutylammomium bromide; sodium hydroxide / toluene; water / 16 h / 20 °C

3.1: copper(l) cyanide; TurboGrignard / tetrahydrofuran / 1 h / 0 - 20 °C

4.1: ozone / dichloromethane; methanol / 1 h / -78 °C

4.2: 16 h / -78 - 20 °C

5.1: tetrahydrofuran / 16 h / -78 - 20 °C

With TurboGrignard; tetrabutylammomium bromide; copper(l) cyanide; ozone; lithium chloride; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; dimethyl sulfoxide; toluene; 1.1: |Krapcho Dealkoxycarbonylation / 5.1: |Grignard Reaction;
DOI:10.1016/j.bmcl.2014.05.082

Reference yield:

: 188347-48-0
2-(3,5-dibromophenyl)acetonitrile

: 1629023-35-3
C₁₅H₁₆BrNO

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutylammomium bromide; sodium hydroxide / toluene; water / 16 h / 20 °C

2.1: copper(l) cyanide; TurboGrignard / tetrahydrofuran / 1 h / 0 - 20 °C

3.1: ozone / dichloromethane; methanol / 1 h / -78 °C

3.2: 16 h / -78 - 20 °C

4.1: tetrahydrofuran / 16 h / -78 - 20 °C

With TurboGrignard; tetrabutylammomium bromide; copper(l) cyanide; ozone; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; toluene; 4.1: |Grignard Reaction;
DOI:10.1016/j.bmcl.2014.05.082