Re(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Re(CO)3(C₆H₅CH₂CN)3ClO₄

Base Information

Chemical Name:Re(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Re(CO)3(C₆H₅CH₂CN)3ClO₄
CAS No.:90364-04-8
Molecular Formula:C₂₇H₂₁N₃O₃Re*ClO₄
Molecular Weight:721.14
Hs Code.:

Re(CO)3(C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>CN)3<sup>(1+)</sup>*ClO<sub>4</sub><sup>(1-)</sup>=Re(CO)3(C<sub>6</sub>H<sub>5</sub>CH<sub>2</sub>CN)3ClO<sub>4</sub>

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Suppliers and Price of Re(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Re(CO)3(C₆H₅CH₂CN)3ClO₄

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Chemical Property of Re(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Re(CO)3(C₆H₅CH₂CN)3ClO₄

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Technology Process of Re(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Re(CO)3(C₆H₅CH₂CN)3ClO₄

There total 1 articles about Re(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Re(CO)3(C₆H₅CH₂CN)3ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 14220-21-4
rhenium(I) pentacarbonyl bromide

: silver perchlorate

: 140-29-4
phenylacetonitrile

: 90364-04-8
Re(CO)3(C₆H₅CH₂CN)3⁽¹⁺⁾*ClO₄^(1-)=Re(CO)3(C₆H₅CH₂CN)3ClO₄

Guidance literature:: In di-isopropyl ether; byproducts: AgBr; a mixt. of Re complex, AgClO4 and PhCH2CN in di-isopropyl ether refluxing for 20 h under dry N2, AgBr removing, ppt. sepg. off after standing for a few days at room temp.; identified by elem. anal. and NMR spectrum;
DOI:10.1016/S0277-5387(00)88120-6