4,4'-bis-(<3,3-(2)H2>n-octyloxy)azoxybenzene

Base Information

Chemical Name:4,4'-bis-(<3,3-(2)H2>n-octyloxy)azoxybenzene
CAS No.:86412-18-2
Molecular Formula:C₂₈H₄₂N₂O₃
Molecular Weight:458.621
Hs Code.:

Synonyms:

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Chemical Property of 4,4'-bis-(<3,3-(2)H2>n-octyloxy)azoxybenzene

Chemical Property:

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Technology Process of 4,4'-bis-(<3,3-(2)H2>n-octyloxy)azoxybenzene

There total 7 articles about 4,4'-bis-(<3,3-(2)H2>n-octyloxy)azoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 86412-17-1
<3,3-(2)H2>octyl bromide

: 15596-57-3,117823-25-3
4,4'-dihydroxyazoxybenzene

: 86412-18-2
4,4'-bis-(<3,3-(2)H2>n-octyloxy)azoxybenzene

Guidance literature:: With potassium carbonate; In cyclohexanone;

Reference yield:

: 78904-38-8
1-bromo-1,1-dideuteriohexane

: 86412-18-2
4,4'-bis-(<3,3-(2)H2>n-octyloxy)azoxybenzene

Guidance literature:: Multi-step reaction with 5 steps

1: 49 percent / sodium / ethanol

2: 1.) sodium, ethanol, 2.) water, 3.) phosphorus trichloride

3: LiAlH₄ / diethyl ether

4: 62.5 percent / hydrobromic acid, conc. sulphuric acid

5: 10 percent / potassium carbonate / cyclohexanone

With lithium aluminium tetrahydride; ethanol; sulfuric acid; water; hydrogen bromide; sodium; potassium carbonate; phosphorus trichloride; In diethyl ether; ethanol; cyclohexanone;

Reference yield:

: 52598-04-6
1-<1,1-(2)H2>hexanol

: 86412-18-2
4,4'-bis-(<3,3-(2)H2>n-octyloxy)azoxybenzene

Guidance literature:: Multi-step reaction with 6 steps

1: hydrobromic acid, conc. sulphuric acid / 6 h / Heating

2: 49 percent / sodium / ethanol

3: 1.) sodium, ethanol, 2.) water, 3.) phosphorus trichloride

4: LiAlH₄ / diethyl ether

5: 62.5 percent / hydrobromic acid, conc. sulphuric acid

6: 10 percent / potassium carbonate / cyclohexanone

With lithium aluminium tetrahydride; ethanol; sulfuric acid; water; hydrogen bromide; sodium; potassium carbonate; phosphorus trichloride; In diethyl ether; ethanol; cyclohexanone;