Technology Process of C47H71N11O24
There total 4 articles about C47H71N11O24 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol;
In
dimethyl sulfoxide;
at 20 ℃;
for 12h;
Molecular sieve;
DOI:10.1021/ja110115a
- Guidance literature:
-
Multi-step reaction with 4 steps
1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 12 h / 20 °C / Inert atmosphere
2: N-ethyl-N,N-diisopropylamine; HATU; (2,4,6-trimethoxyphenyl)methanethiol / N,N-dimethyl-formamide / Inert atmosphere
3: chlorotriisopropylsilane; water; trifluoroacetic acid; phenol / 1 h / Inert atmosphere
4: benzotriazol-1-ol / dimethyl sulfoxide / 12 h / 20 °C / Molecular sieve
With
chlorotriisopropylsilane; palladium 10% on activated carbon; water; hydrogen; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; (2,4,6-trimethoxyphenyl)methanethiol; phenol;
In
dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/ja110115a
- Guidance literature:
-
Multi-step reaction with 3 steps
1: N-ethyl-N,N-diisopropylamine; HATU; (2,4,6-trimethoxyphenyl)methanethiol / N,N-dimethyl-formamide / Inert atmosphere
2: chlorotriisopropylsilane; water; trifluoroacetic acid; phenol / 1 h / Inert atmosphere
3: benzotriazol-1-ol / dimethyl sulfoxide / 12 h / 20 °C / Molecular sieve
With
chlorotriisopropylsilane; water; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine; HATU; trifluoroacetic acid; (2,4,6-trimethoxyphenyl)methanethiol; phenol;
In
dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1021/ja110115a
