closo-1-Me-2-(2'-hydroxycyclohexyl)-1,2-C₂B₁₀H₁₀

Base Information

Chemical Name:closo-1-Me-2-(2'-hydroxycyclohexyl)-1,2-C₂B₁₀H₁₀
CAS No.:848137-81-5
Molecular Formula:C₉H₂₄B₁₀O
Molecular Weight:256.399
Hs Code.:

closo-1-Me-2-(2'-hydroxycyclohexyl)-1,2-C<sub>2</sub>B<sub>10</sub>H<sub>10</sub>

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Chemical Property of closo-1-Me-2-(2'-hydroxycyclohexyl)-1,2-C₂B₁₀H₁₀

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Technology Process of closo-1-Me-2-(2'-hydroxycyclohexyl)-1,2-C₂B₁₀H₁₀

There total 1 articles about closo-1-Me-2-(2'-hydroxycyclohexyl)-1,2-C₂B₁₀H₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 109-72-8,29786-93-4
n-butyllithium

: 16872-10-9
1-methyl-o-carborane

: 286-20-4
cyclohexane-1,2-epoxide

: 848137-81-5
closo-1-Me-2-(2'-hydroxycyclohexyl)-1,2-C₂B₁₀H₁₀

Guidance literature:: In diethyl ether; hexane; benzene; under inert atm. to soln. 1-Me-1,2-C2B10H11 in Et2O-benzene at -78°C soln. n-BuLi in n-hexane was added, stirred for 0.5 h, allowed to warm to room temp., stirred for 4 h, cyclohexene oxide was added at 0°C, stirred at room temp. for 6 h; water was added, org. phase was dried over MgSO4, solvent was removed invacuo, residue was recrystd. from n-hexane; elem. anal.;
DOI:10.1016/j.jorganchem.2005.01.047

Reference yield: 82.0%

: 848137-81-5
closo-1-Me-2-(2'-hydroxycyclohexyl)-1,2-C₂B₁₀H₁₀

: potassium hydroxide

: K[nido-7-Me-8-(2'-hydroxycyclohexyl)-7,8-C₂B₉H₁₀]

Guidance literature:: In ethanol; under inert atm. soln. closo-1-Me-2-(2'-hydroxycyclohexyl)-1,2-C2B10H10 in ethanolic KOH was heated at reflux for 16 h; react. mixt. was cooled to room temp. and neutralized with aq. HCl, solvent was removed in vacuo, residue was extd. with THF, soln. was filteredand dried in vacuo; elem. anal.;
DOI:10.1016/j.jorganchem.2005.01.047