C₄₅H₆₃N₅O₂₃

Base Information

Chemical Name:C₄₅H₆₃N₅O₂₃
CAS No.:129415-19-6
Molecular Formula:C₄₅H₆₃N₅O₂₃
Molecular Weight:1042.01
Hs Code.:

C<sub>45</sub>H<sub>63</sub>N<sub>5</sub>O<sub>23</sub>

Synonyms:

Suppliers and Price of C₄₅H₆₃N₅O₂₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₅H₆₃N₅O₂₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₅H₆₃N₅O₂₃

There total 8 articles about C₄₅H₆₃N₅O₂₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 73724-48-8
N-(fluoren-9-ylmethoxycarbonyl)-L-threonine benzyl ester

: 129415-19-6
C₄₅H₆₃N₅O₂₃

Guidance literature:: Multi-step reaction with 6 steps

1: 1. Ag₂CO₃, Drierite, molecular sieves (3 Angstroem) 2. AgClO₄ / 1. CH₂Cl₂, toluene, -5 deg C, 30 min 2. 20 h, room temperature

2: 1. NaBH₄ 2. pyridine / 1. NiCl₂*6H₂O, boric acid / 1. EtOH 2. 2 h

3: morpholine / 0.5 h / Ambient temperature

4: 81 percent / ethyl 2-ethoxy-1,2-dihydroquinoline-1-carboxylate / CH₂Cl₂ / 120 h

5: CH₂Cl₂ / 12 h / Ambient temperature

6: morpholine / CH₂Cl₂ / 1 h

With morpholine; pyridine; calcium sulfate; sodium tetrahydroborate; 3 A molecular sieve; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; silver carbonate; boric acid; nickel dichloride; In dichloromethane;
DOI:10.1016/0008-6215(90)84081-5

Reference yield:

: 100938-55-4
N-(9H-fluorene-9-yl)-methoxycarbonyl-O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)-L-threonine benzyl ester

: 129415-19-6
C₄₅H₆₃N₅O₂₃

Guidance literature:: Multi-step reaction with 5 steps

1: 1. NaBH₄ 2. pyridine / 1. NiCl₂*6H₂O, boric acid / 1. EtOH 2. 2 h

2: morpholine / 0.5 h / Ambient temperature

3: 81 percent / ethyl 2-ethoxy-1,2-dihydroquinoline-1-carboxylate / CH₂Cl₂ / 120 h

4: CH₂Cl₂ / 12 h / Ambient temperature

5: morpholine / CH₂Cl₂ / 1 h

With morpholine; pyridine; sodium tetrahydroborate; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; boric acid; nickel dichloride; In dichloromethane;
DOI:10.1016/0008-6215(90)84081-5

Reference yield:

: 100929-00-8
benzyl O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)-N-[(9H-fluoren-9-ylmethoxy)carbonyl]-L-serinate

: 129415-19-6
C₄₅H₆₃N₅O₂₃

Guidance literature:: Multi-step reaction with 7 steps

1: 1. NaBH₄ 2. pyridine / 1. NiCl₂*6H₂O, boric acid / 1. EtOH 2. 2 h

2: morpholine / 0.5 h / Ambient temperature

3: 75 percent / ethyl 2-ethoxy-1,2-dihydroquinoline-1-carboxylate / CH₂Cl₂ / 72 h

4: H₂ / 5percent Pd-C / methanol / 15 h

5: 81 percent / ethyl 2-ethoxy-1,2-dihydroquinoline-1-carboxylate / CH₂Cl₂ / 120 h

6: CH₂Cl₂ / 12 h / Ambient temperature

7: morpholine / CH₂Cl₂ / 1 h

With morpholine; pyridine; sodium tetrahydroborate; hydrogen; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; palladium on activated charcoal; boric acid; nickel dichloride; In methanol; dichloromethane;
DOI:10.1016/0008-6215(90)84081-5