(-)-[4aS-(4aα,6β,8aR*)]-4a,5,9,10,11,12-hexahydro-3-[13CD3]-methoxy-11-methyl-6H-benzofuro[3a,3,2-e,f][2]-benzazepin-3,6-diol hydrobromide

Base Information

• Chemical Name: (-)-[4aS-(4aα,6β,8aR*)]-4a,5,9,10,11,12-hexahydro-3-[13CD3]-methoxy-11-methyl-6H-benzofuro[3a,3,2-e,f][2]-benzazepin-3,6-diol hydrobromide
• CAS No.: 2140262-53-7
• Molecular Formula: BrH*C₁₇H₂₁NO₃
• Molecular Weight: 372.236
• Mol file: 2140262-53-7.mol

Synonyms:

Chemical Property of (-)-[4aS-(4aα,6β,8aR*)]-4a,5,9,10,11,12-hexahydro-3-[13CD3]-methoxy-11-methyl-6H-benzofuro[3a,3,2-e,f][2]-benzazepin-3,6-diol hydrobromide

Chemical Property:

Purity/Quality:

95% by CP; 98% atom D ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (-)-[4aS-(4aα,6β,8aR*)]-4a,5,9,10,11,12-hexahydro-3-[13CD3]-methoxy-11-methyl-6H-benzofuro[3a,3,2-e,f][2]-benzazepin-3,6-diol hydrobromide

There total 1 articles about (-)-[4aS-(4aα,6β,8aR*)]-4a,5,9,10,11,12-hexahydro-3-[13CD3]-methoxy-11-methyl-6H-benzofuro[3a,3,2-e,f][2]-benzazepin-3,6-diol hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.1%

[13C,2H4]methyl alcohol (32479-98-4) + (-)-[4aS-(4aα,6β,8aR*)]-4a,5,9,10,11,12-hexahydro-11-methyl-6H-benzofuro[3a,3,2-e,f][2]-benzazepin-3,6-diol hydrochloride → (-)-[4aS-(4aα,6β,8aR*)]-4a,5,9,10,11,12-hexahydro-3-[13CD3]-methoxy-11-methyl-6H-benzofuro[3a,3,2-e,f][2]-benzazepin-3,6-diol hydrobromide (2140262-53-7)

Guidance literature:

[¹³C,²H₄]methyl alcohol; (-)-[4aS-(4aα,6β,8aR*)]-4a,5,9,10,11,12-hexahydro-11-methyl-6H-benzofuro[3a,3,2-e,f][2]-benzazepin-3,6-diol hydrochloride; With di-isopropyl azodicarboxylate; polymer bound triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 20h;

With hydrogen bromide; In ethanol; for 1.5h;

DOI:10.1002/jlcr.589

upstream raw materials:

[¹³C,²H₄]methyl alcohol