Technology Process of C37H44N7O8S(1+)*I(1-)
There total 5 articles about C37H44N7O8S(1+)*I(1-) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 3 h / 0 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / acetone / 0.25 h / 0 °C
3: sodium iodide / acetone / 1 h / 20 °C
4: acetonitrile / 6 h / 20 °C / Inert atmosphere
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium iodide;
In
N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ja208290f
- Guidance literature:
-
Multi-step reaction with 4 steps
1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 3 h / 0 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid / acetone / 0.25 h / 0 °C
3: sodium iodide / acetone / 1 h / 20 °C
4: acetonitrile / 6 h / 20 °C / Inert atmosphere
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; 3-chloro-benzenecarboperoxoic acid; sodium iodide;
In
N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/ja208290f
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium iodide / acetone / 1 h / 20 °C
2: acetonitrile / 6 h / 20 °C / Inert atmosphere
With
sodium iodide;
In
acetone; acetonitrile;
DOI:10.1021/ja208290f
