(-)-2,3,4,5,6-pentakis-O-benzyl myo-inositol bis(2-cyanoethyl) phosphorothioate

Base Information

• Chemical Name: (-)-2,3,4,5,6-pentakis-O-benzyl myo-inositol bis(2-cyanoethyl) phosphorothioate
• CAS No.: 135363-27-8
• Molecular Formula: C₄₇H₄₉N₂O₈PS
• Molecular Weight: 832.954

Synonyms:

Chemical Property of (-)-2,3,4,5,6-pentakis-O-benzyl myo-inositol bis(2-cyanoethyl) phosphorothioate

Chemical Property:

Purity/Quality:

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Technology Process of (-)-2,3,4,5,6-pentakis-O-benzyl myo-inositol bis(2-cyanoethyl) phosphorothioate

There total 21 articles about (-)-2,3,4,5,6-pentakis-O-benzyl myo-inositol bis(2-cyanoethyl) phosphorothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Phosphorous acid bis-(2-cyano-ethyl) ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl ester → (+)-2,3,4,5,6-pentakis-O-benzyl myo-inositol bis(2-cyanoethyl) phosphorothioate (135363-27-8,135415-98-4,135415-99-5)

Guidance literature:

With sulfur; In pyridine; for 0.25h; Yield given;

DOI:10.1016/S0040-4020(01)80912-1

Reference yield:

Phosphorous acid bis-(2-cyano-ethyl) ester (1S,2S,3R,4S,5S,6S)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl ester → (-)-2,3,4,5,6-pentakis-O-benzyl myo-inositol bis(2-cyanoethyl) phosphorothioate (135363-27-8,135415-98-4,135415-99-5)

Guidance literature:

With sulfur; In pyridine; for 0.25h; Yield given;

DOI:10.1016/S0040-4020(01)80912-1

Reference yield:

Phosphorous acid bis-(2-cyano-ethyl) ester (1S,2R,3R,4S,5S,6R)-2,3,4,5,6-pentakis-benzyloxy-cyclohexyl ester → (+/-)-2,3,4,5,6-pentakis-O-benzyl myo-inositol bis(2-cyanoethyl) phosphorothioate (135363-27-8,135415-98-4,135415-99-5)

Guidance literature:

With sulfur; In pyridine; for 0.25h; Yield given;

DOI:10.1016/S0040-4020(01)80912-1

upstream raw materials:

(+/-)-1-O-allyl-3,4,5,6-tetrakis-O-benzyl myo-inositol

(+/-)-1-O-allyl-2,3,4,5,6-pentakis-O-benzyl myo-inositol

rac-1,4,5,6-tetra-O-benzyl-myo-inositol

DL-2,3,4,5,6-penta-O-benzyl-myo-inositol

Downstream raw materials:

(+/-) myo-inositol 1-phosphorothioate biscyclohexylammonium salt

inositol 1-phosphorothioate

(D)-myo-inositol 1-phosphorothioate biscyclohexylammonium salt

Thiophosphoric acid O-((1S,2S,3R,4S,5S,6S)-2,3,4,5,6-pentahydroxy-cyclohexyl) ester

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