MoO₂⁽²⁺⁾*C₆H₄(O)(CCH₃N(C₆H₄O))^(2-)=MoO₂(C₆H₄(O)(CCH₃N(C₆H₄O)))

Base Information

• Chemical Name: MoO₂⁽²⁺⁾*C₆H₄(O)(CCH₃N(C₆H₄O))^(2-)=MoO₂(C₆H₄(O)(CCH₃N(C₆H₄O)))
• CAS No.: 75790-25-9
• Molecular Formula: C₁₄H₁₁NO₂*MoO₂
• Molecular Weight: 353.186
• Mol file: 75790-25-9.mol

Synonyms:

Chemical Property of MoO₂⁽²⁺⁾*C₆H₄(O)(CCH₃N(C₆H₄O))^(2-)=MoO₂(C₆H₄(O)(CCH₃N(C₆H₄O)))

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of MoO₂⁽²⁺⁾*C₆H₄(O)(CCH₃N(C₆H₄O))^(2-)=MoO₂(C₆H₄(O)(CCH₃N(C₆H₄O)))

There total 2 articles about MoO₂⁽²⁺⁾*C₆H₄(O)(CCH₃N(C₆H₄O))^(2-)=MoO₂(C₆H₄(O)(CCH₃N(C₆H₄O))) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

MoO2(C6H4(O)(CCH3N(C6H4O)))(CH3CH2OH) (64722-32-3) → MoO2(2+)*C6H4(O)(CCH3N(C6H4O))(2-)=MoO2(C6H4(O)(CCH3N(C6H4O))) (75790-25-9)

Guidance literature:

In neat (no solvent); complex was dried at 100°C under vac.;

DOI:10.1021/ic50217a005

Reference yield: 55.0%

MoO2(C6H4(O)(CCH3N(C6H4O)))(H2O) (75790-21-5) → MoO2(2+)*C6H4(O)(CCH3N(C6H4O))(2-)=MoO2(C6H4(O)(CCH3N(C6H4O))) (75790-25-9)

Guidance literature:

In neat (no solvent); complex was dried at 80°C under vac.;

DOI:10.1021/ic50217a005

Reference yield:

MoO2(2+)*C6H4(O)(CCH3N(C6H4O))(2-)=MoO2(C6H4(O)(CCH3N(C6H4O))) (75790-25-9) → MoO2(C6H4(O)(CCH3N(C6H4O)))((C6H5)3P) (75790-24-8)

Guidance literature:

With triphenylphosphine; In dichloromethane; to complex in CH2Cl2 ligand was added with stirring, soln. was heated at reflux under N2 for ca. 1 h on water bath; soln. was cooled, solid was filtered, washed with CH2Cl2, dried in vac.;

DOI:10.1021/ic50217a005

upstream raw materials:

MoO₂(C₆H₄(O)(CCH₃N(C₆H₄O)))(CH₃CH₂OH)

MoO₂(C₆H₄(O)(CCH₃N(C₆H₄O)))(H₂O)

Downstream raw materials:

MoO₂(C₆H₄(O)(CCH₃N(C₆H₄O)))((C₆H₅)3P)

MoO₂(C₆H₄(O)(CCH₃N(C₆H₄O)))((C₆H₅)CHO)