Rh₂Cl₂(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)*99CH₂Cl₂=Rh₂Cl₂(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2BF₄*99CH₂Cl₂

Base Information

• Chemical Name: Rh₂Cl₂(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)*99CH₂Cl₂=Rh₂Cl₂(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2BF₄*99CH₂Cl₂
• CAS No.: 89321-58-4
• Molecular Formula: BF₄*(x)CH₂Cl₂*C₅₃H₅₀Cl₂NP₄Rh₂S

Synonyms:

Chemical Property of Rh₂Cl₂(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)*99CH₂Cl₂=Rh₂Cl₂(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2BF₄*99CH₂Cl₂

Chemical Property:

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Safty Information:

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Technology Process of Rh₂Cl₂(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)*99CH₂Cl₂=Rh₂Cl₂(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2BF₄*99CH₂Cl₂

There total 1 articles about Rh₂Cl₂(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)*99CH₂Cl₂=Rh₂Cl₂(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2BF₄*99CH₂Cl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Rh2Cl2(CO)(SCN(CH3)2)((C6H5)2PCH2P(C6H5)2)2(1+)*BF4(1-)*99CH2Cl2=Rh2Cl2(CO)(SCN(CH3)2)((C6H5)2PCH2P(C6H5)2)2BF4*99CH2Cl2 → Rh2Cl2(SCN(CH3)2)((C6H5)2PCH2P(C6H5)2)2(1+)*BF4(1-)*99CH2Cl2=Rh2Cl2(SCN(CH3)2)((C6H5)2PCH2P(C6H5)2)2BF4*99CH2Cl2 (89321-58-4)

Guidance literature:

With trimethylamine oxide dihydrate; In dichloromethane; Rh-complex and Me3NO*2H2O were dissolved in CH2Cl2 under N2, soln. was stirred at room temp. for 1 h; soln. was concd., Et2O added, filtered in air, ppt. was washed with MeOH-Et2O, Et2O, recrystd. from CH2Cl2-Et2O; elem. anal. for the solvate with 0.4 equiv of CH2Cl2;

Reference yield: 70.0%

methyl isocyanate (593-75-9,685498-28-6) + Rh2Cl2(SCN(CH3)2)((C6H5)2PCH2P(C6H5)2)2(1+)*BF4(1-)*99CH2Cl2=Rh2Cl2(SCN(CH3)2)((C6H5)2PCH2P(C6H5)2)2BF4*99CH2Cl2 (89321-58-4) → Rh2Cl2(CNCH3)(SCN(CH3)2)((C6H5)2PCH2P(C6H5)2)2(1+)*BF4(1-)=Rh2Cl2(CNCH3)(SCN(CH3)2)((C6H5)2PCH2P(C6H5)2)2BF4 (89321-60-8)

Guidance literature:

In dichloromethane; MeNC was added under N2 to a CH2Cl2 soln. of Rh-complex, mixt. was stirred for 30 min; concd., Et2O was added, ppt. isolated by filtration in air, washed withEt2O;

Reference yield:

Rh2Cl2(SCN(CH3)2)((C6H5)2PCH2P(C6H5)2)2(1+)*BF4(1-)*99CH2Cl2=Rh2Cl2(SCN(CH3)2)((C6H5)2PCH2P(C6H5)2)2BF4*99CH2Cl2 (89321-58-4) → Rh2(CO)2(SCN(CH3)2)((C6H5)2PCH2P(C6H5)2)2(1+)*BF4(1-)=Rh2(CO)2(SCN(CH3)2)((C6H5)2PCH2P(C6H5)2)2BF4 (89321-64-2)

Guidance literature:

Multi-step reaction with 2 steps

1: carbon monoxide / dichloromethane

2: [Et₄N][BH₄]; CO / acetonitrile

With carbon monoxide; [Et₄N][BH₄]; CO; In dichloromethane; acetonitrile;

Downstream raw materials:

Rh₂Cl₂(CNCH₃)(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)=Rh₂Cl₂(CNCH₃)(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2BF₄

Rh₂(CO)(CH₃CN)(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)=Rh₂(CO)(CH₃CN)(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2BF₄

Rh₂(CO)(C₄H₈O)(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)=Rh₂(CO)(C₄H₈O)(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2BF₄

Rh₂(CO)2(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2⁽¹⁺⁾*BF₄^(1-)=Rh₂(CO)2(SCN(CH₃)2)((C₆H₅)2PCH₂P(C₆H₅)2)2BF₄

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