[C₆H₄C(O)N(CH(CH₃)2)2]2BF

Base Information

• Chemical Name: [C₆H₄C(O)N(CH(CH₃)2)2]2BF
• CAS No.: 870530-92-0
• Molecular Formula: C₂₆H₃₆BFN₂O₂
• Molecular Weight: 438.393
• Mol file: 870530-92-0.mol

Synonyms:

Chemical Property of [C₆H₄C(O)N(CH(CH₃)2)2]2BF

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [C₆H₄C(O)N(CH(CH₃)2)2]2BF

There total 2 articles about [C₆H₄C(O)N(CH(CH₃)2)2]2BF which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

potassium hydrogen bifluoride + [C6H4C(O)N(CH(CH3)2)2]2B(1+)*Cl(1-)=[[C6H4C(O)N(CH(CH3)2)2]2B]Cl (870530-88-4) → [C6H4C(O)N(CH(CH3)2)2]2BF (870530-92-0)

Guidance literature:

In methanol; water; using Teflon vessel; to stirred soln. of borinate in MeOH added KHF2 dissolved in min. amt. of H2O; after 40 min ppt. filtered; washed (cold MeOH); dried; recrystd. (MeCN);

DOI:10.1016/j.jorganchem.2005.07.108

Reference yield:

N,N-diisopropyl benzamide (20383-28-2) → [C6H4C(O)N(CH(CH3)2)2]2BF (870530-92-0)

Guidance literature:

Multi-step reaction with 2 steps

1: tetramethylethylenediamine; n-butyllithium or sec-buthyllithium / tetrahydrofuran; hexane

2: water; methanol

With tetramethylethylenediamine; n-butyllithium or sec-buthyllithium; In tetrahydrofuran; methanol; hexane; water;

DOI:10.1016/j.jorganchem.2005.07.108

upstream raw materials:

[C₆H₄C(O)N(CH(CH₃)2)2]2B⁽¹⁺⁾*Cl^(1-)=[[C₆H₄C(O)N(CH(CH₃)2)2]2B]Cl

N,N-diisopropyl benzamide