(1S,2R,3R,4R,6S,Z)-4-[3-{2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl}-1-{(2-methoxyethoxy)methoxy}-2-propen-2-yl]-2,3-epoxy-1-methylcyclohexan-1,6-diol

Base Information

Chemical Name:(1S,2R,3R,4R,6S,Z)-4-[3-{2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl}-1-{(2-methoxyethoxy)methoxy}-2-propen-2-yl]-2,3-epoxy-1-methylcyclohexan-1,6-diol
CAS No.:1115267-10-1
Molecular Formula:C₄₃H₅₂O₈Si
Molecular Weight:724.967
Hs Code.:

(1S,2R,3R,4R,6S,Z)-4-[3-{2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl}-1-{(2-methoxyethoxy)methoxy}-2-propen-2-yl]-2,3-epoxy-1-methylcyclohexan-1,6-diol

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Chemical Property of (1S,2R,3R,4R,6S,Z)-4-[3-{2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl}-1-{(2-methoxyethoxy)methoxy}-2-propen-2-yl]-2,3-epoxy-1-methylcyclohexan-1,6-diol

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Technology Process of (1S,2R,3R,4R,6S,Z)-4-[3-{2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl}-1-{(2-methoxyethoxy)methoxy}-2-propen-2-yl]-2,3-epoxy-1-methylcyclohexan-1,6-diol

There total 1 articles about (1S,2R,3R,4R,6S,Z)-4-[3-{2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl}-1-{(2-methoxyethoxy)methoxy}-2-propen-2-yl]-2,3-epoxy-1-methylcyclohexan-1,6-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1115267-09-8
(1R,2S,4R,Z)-4-[3-{2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl}-1-{(2-methoxyethoxy)methoxy}-2-propen-2-yl]-1-methyl-5-cyclohexen-1,2-diol

: 1115267-10-1
(1S,2R,3R,4R,6S,Z)-4-[3-{2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl}-1-{(2-methoxyethoxy)methoxy}-2-propen-2-yl]-2,3-epoxy-1-methylcyclohexan-1,6-diol

: 1115267-26-9
C₄₃H₅₂O₉Si

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -30 ℃; for 16h;
DOI:10.1016/j.tet.2008.11.055

Reference yield:

: 1115267-10-1
(1S,2R,3R,4R,6S,Z)-4-[3-{2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl}-1-{(2-methoxyethoxy)methoxy}-2-propen-2-yl]-2,3-epoxy-1-methylcyclohexan-1,6-diol

: 1115267-12-3
(2S,6R,Z)-t-4-[3-{2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl}-1-{(2-methoxyethoxy)methoxy}-2-propen-2-yl]-1-methylcyclohexan-r-1,c-2,c-6-triol

Guidance literature:: (1S,2R,3R,4R,6S,Z)-4-[3-{2-benzyloxy-4-(tert-butyldiphenylsilanyloxy)phenyl}-1-{(2-methoxyethoxy)methoxy}-2-propen-2-yl]-2,3-epoxy-1-methylcyclohexan-1,6-diol; With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 5h;

With hydrogenchloride; In tetrahydrofuran; water; Cooling with ice;
DOI:10.1016/j.tet.2008.11.055