p-Isothiocyanatophenyl urethane

Base Information

Chemical Name:p-Isothiocyanatophenyl urethane
CAS No.:78889-13-1
Molecular Formula:C₁₀H₁₀N₂O₂S
Molecular Weight:222.268
Hs Code.:

Synonyms:

Suppliers and Price of p-Isothiocyanatophenyl urethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-Isothiocyanatophenyl urethane

Chemical Property:

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Technology Process of p-Isothiocyanatophenyl urethane

There total 1 articles about p-Isothiocyanatophenyl urethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 463-71-8
thiophosgene

: 57399-97-0
N-(4-aminophenyl)carbamic acid ethyl ester

: 78889-13-1
p-Isothiocyanatophenyl urethane

Guidance literature:: In 1,4-dioxane; water; 1.) 15 deg C , 2 h , 2.) RT , overnight;

Reference yield:

: 78889-13-1
p-Isothiocyanatophenyl urethane

: 26328-53-0,100990-46-3
Amoscanate

Guidance literature:: Multi-step reaction with 3 steps

1: 0.8 g / PCl₅ / chlorobenzene / 2 h / Heating

2: 6.7 g / Pyridine / benzene / 3 h / 50 - 60 °C

3: 0.1 g / anhydrous K₂CO₃ / nitrobenzene / 3 h / 190 °C / Further catalysts

With pyridine; phosphorus pentachloride; potassium carbonate; In nitrobenzene; chlorobenzene; benzene;

Reference yield:

: 78889-13-1
p-Isothiocyanatophenyl urethane

: 78889-14-2
(4-Isothiocyanato-phenyl)-carbamic acid 4-nitro-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 0.8 g / PCl₅ / chlorobenzene / 2 h / Heating

2: 6.7 g / Pyridine / benzene / 3 h / 50 - 60 °C

With pyridine; phosphorus pentachloride; In chlorobenzene; benzene;