C₃₃H₄₂N₂O₈

Base Information

Chemical Name:C₃₃H₄₂N₂O₈
CAS No.:99602-75-2
Molecular Formula:C₃₃H₄₂N₂O₈
Molecular Weight:594.705
Hs Code.:

C<sub>33</sub>H<sub>42</sub>N<sub>2</sub>O<sub>8</sub>

Synonyms:

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Chemical Property of C₃₃H₄₂N₂O₈

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Technology Process of C₃₃H₄₂N₂O₈

There total 10 articles about C₃₃H₄₂N₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2199-44-2
3,5-dimethyl-2-ethoxycarbonyl-1H-pyrrole

: 99602-75-2
C₃₃H₄₂N₂O₈

Guidance literature:: Multi-step reaction with 7 steps

1: 95 percent / phenylmethanol / 0.5 h / 209 °C

2: 77 percent / SnCl₄ / CH₂Cl₂ / 0.25 h

3: 81 percent / sodium borohydride, BF₃*Et₂O / tetrahydrofuran / 0 deg C 15 min, methanol reflux 15 min

4: H₂ / 10percent Pd/C / tetrahydrofuran / Ambient temperature

5: 67 percent / dicyclohexyl-carbodi-imide / tetrahydrofuran / 16 h / 20 °C

6: 72 percent / lead tetra-acetate / 1 h

7: toluene-p-sulphonic acid / CH₂Cl₂ / 1.5 h / Ambient temperature

With lead(IV) acetate; sodium tetrahydroborate; boron trifluoride diethyl etherate; hydrogen; tin(IV) chloride; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; benzyl alcohol;

Reference yield:

: 40236-19-9
benzyl 3,5-dimethylpyrrole-2-carboxylate

: 99602-75-2
C₃₃H₄₂N₂O₈

Guidance literature:: Multi-step reaction with 6 steps

1: 77 percent / SnCl₄ / CH₂Cl₂ / 0.25 h

2: 81 percent / sodium borohydride, BF₃*Et₂O / tetrahydrofuran / 0 deg C 15 min, methanol reflux 15 min

3: H₂ / 10percent Pd/C / tetrahydrofuran / Ambient temperature

4: 67 percent / dicyclohexyl-carbodi-imide / tetrahydrofuran / 16 h / 20 °C

5: 72 percent / lead tetra-acetate / 1 h

6: toluene-p-sulphonic acid / CH₂Cl₂ / 1.5 h / Ambient temperature

With lead(IV) acetate; sodium tetrahydroborate; boron trifluoride diethyl etherate; hydrogen; tin(IV) chloride; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;

Reference yield:

: 99602-58-1
benzyl 3-(3-methoxycarbonylpropionyl)-2,4-dimethylpyrrole-5-carboxylate

: 99602-75-2
C₃₃H₄₂N₂O₈

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / sodium borohydride, BF₃*Et₂O / tetrahydrofuran / 0 deg C 15 min, methanol reflux 15 min

2: H₂ / 10percent Pd/C / tetrahydrofuran / Ambient temperature

3: 67 percent / dicyclohexyl-carbodi-imide / tetrahydrofuran / 16 h / 20 °C

4: 72 percent / lead tetra-acetate / 1 h

5: toluene-p-sulphonic acid / CH₂Cl₂ / 1.5 h / Ambient temperature

With lead(IV) acetate; sodium tetrahydroborate; boron trifluoride diethyl etherate; hydrogen; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; dichloromethane;