cyclopent-3-enyl-(5-hydroxy-2-methoxy-phenyl)-methanone

Base Information

Chemical Name:cyclopent-3-enyl-(5-hydroxy-2-methoxy-phenyl)-methanone
CAS No.:861220-61-3
Molecular Formula:C₁₃H₁₄O₃
Molecular Weight:218.252
Hs Code.:

Synonyms:

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Chemical Property of cyclopent-3-enyl-(5-hydroxy-2-methoxy-phenyl)-methanone

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Technology Process of cyclopent-3-enyl-(5-hydroxy-2-methoxy-phenyl)-methanone

There total 1 articles about cyclopent-3-enyl-(5-hydroxy-2-methoxy-phenyl)-methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 248275-70-9
cyclopent-3-enecarboxylic acid methoxy-methyl-amide

: 861220-61-3
cyclopent-3-enyl-(5-hydroxy-2-methoxy-phenyl)-methanone

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at -78 - 20 ℃;
DOI:10.1016/j.bmcl.2005.04.036

Reference yield:

: 861220-61-3
cyclopent-3-enyl-(5-hydroxy-2-methoxy-phenyl)-methanone

: 5-phenyl-11-aza-tricyclo[7.3.1.0^2,7]trideca-2⁽⁷⁾,3,5-triene

Guidance literature:: Multi-step reaction with 10 steps

1: BCl₃ / CH₂Cl₂

2: pyridine / CH₂Cl₂

3: Ph₃P(CH₂)3PPh₃; KOAc; Et₃N / Pd(OAc)2 / dimethylformamide / 110 °C

4: 93 percent / N₂H₄; KOH; ethanediol / Heating

5: aq. OsO₄; (CH₂)5NCH₃O / acetone

6: aq. NaIO₄ / 1,2-dichloro-ethane

7: NaBH(OAc)3 / 1,2-dichloro-ethane

8: 94 percent / pyridine / CH₂Cl₂

9: 23 percent / aq. Pd(PPh₃)4; KOAc / ethanol / 18 h / 90 °C

10: NH₄HCO₂ / Pd(OH)2 / methanol / Heating

With pyridine; potassium hydroxide; sodium periodate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; (CH₂)5NCH₃O; Ph₃P(CH₂)3PPh₃; ammonium formate; potassium acetate; boron trichloride; sodium tris(acetoxy)borohydride; ethylene glycol; triethylamine; hydrazine; palladium diacetate; palladium dihydroxide; In methanol; ethanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; 3: Heck reaction / 4: Wolff-Kishner reduction / 9: Suzuki coupling;
DOI:10.1016/j.bmcl.2005.04.036

Reference yield:

: 861220-61-3
cyclopent-3-enyl-(5-hydroxy-2-methoxy-phenyl)-methanone

: 5-(4-methoxy-phenyl)-11-aza-tricyclo[7.3.1.02.7]trideca-2⁽⁷⁾,3,5-triene

Guidance literature:: Multi-step reaction with 10 steps

1: BCl₃ / CH₂Cl₂

2: pyridine / CH₂Cl₂

3: Ph₃P(CH₂)3PPh₃; KOAc; Et₃N / Pd(OAc)2 / dimethylformamide / 110 °C

4: 93 percent / N₂H₄; KOH; ethanediol / Heating

5: aq. OsO₄; (CH₂)5NCH₃O / acetone

6: aq. NaIO₄ / 1,2-dichloro-ethane

7: NaBH(OAc)3 / 1,2-dichloro-ethane

8: 94 percent / pyridine / CH₂Cl₂

9: 23 percent / aq. Pd(PPh₃)4; KOAc / ethanol / 18 h / 90 °C

10: NH₄HCO₂ / Pd(OH)2 / methanol / Heating

With pyridine; potassium hydroxide; sodium periodate; osmium(VIII) oxide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; (CH₂)5NCH₃O; Ph₃P(CH₂)3PPh₃; ammonium formate; potassium acetate; boron trichloride; sodium tris(acetoxy)borohydride; ethylene glycol; triethylamine; hydrazine; palladium diacetate; palladium dihydroxide; In methanol; ethanol; dichloromethane; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone; 3: Heck reaction / 4: Wolff-Kishner reduction / 9: Suzuki coupling;
DOI:10.1016/j.bmcl.2005.04.036