ethyl 1-(2-oxo-2-p-tolylethyl)-3-ferrocenyl-1H-pyrazole-5-carboxylate

Base Information

Chemical Name:ethyl 1-(2-oxo-2-p-tolylethyl)-3-ferrocenyl-1H-pyrazole-5-carboxylate
CAS No.:1184295-28-0
Molecular Formula:C₂₅H₂₄FeN₂O₃
Molecular Weight:456.324
Hs Code.:

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Chemical Property of ethyl 1-(2-oxo-2-p-tolylethyl)-3-ferrocenyl-1H-pyrazole-5-carboxylate

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Technology Process of ethyl 1-(2-oxo-2-p-tolylethyl)-3-ferrocenyl-1H-pyrazole-5-carboxylate

There total 1 articles about ethyl 1-(2-oxo-2-p-tolylethyl)-3-ferrocenyl-1H-pyrazole-5-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: ethyl 3-ferrocenyl-1H-pyrazole-5-carboxylate

: 619-41-0
4-(bromoacetyl)toluene

: 1184295-28-0
ethyl 1-(2-oxo-2-p-tolylethyl)-3-ferrocenyl-1H-pyrazole-5-carboxylate

Guidance literature:: With K₂CO₃; KI; In acetonitrile; (under N2); K2CO3 and KI added to soln. of Fe-complex and ligand in MeCN, refluxed for 4 h, cooled to room temp.; filtered, evapd. under reduced pressure, flash silica gel column chromy.with ethyl acetate/petroleum ether 1:4;
DOI:10.1016/j.molstruc.2009.04.042

Reference yield: 14.0%

: 1184295-28-0
ethyl 1-(2-oxo-2-p-tolylethyl)-3-ferrocenyl-1H-pyrazole-5-carboxylate

: magnesium bromide ethyl etherate

: 1184295-22-4
2-ferrocenyl-6-p-tolyl-4H-pyrazolo[5,1-c][1,4]oxazin-4-one

Guidance literature:: With N,N-diisopropylethylamine; In toluene; (under N2); MgBr2*Et2O added to stirred soln. of Fe-complex and N,N-diisopropylethylamine, refluxed for 4 h, cooled to room temp.; filtered, evapd. under reduced pressure, silica gel column chromy. with CH2Cl2/petroleum ether 1:1;
DOI:10.1016/j.molstruc.2009.04.042