Technology Process of C30H38F2N2O2
There total 14 articles about C30H38F2N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: triethylamine / dichloromethane
2: lithium diisopropyl amide
3: dihydrogen peroxide; lithium hydroxide / tetrahydrofuran; water
4: diphenyl phosphoryl azide; triethylamine / toluene
5: palladium on activated charcoal; hydrogen / methanol
6: sodium tris(acetoxy)borohydride / dichloromethane
7: N,N-dimethyl-formamide / 50 - 60 °C
8: trifluoroacetic acid / water
9: L-Selectride / tetrahydrofuran
With
diphenyl phosphoryl azide; palladium on activated charcoal; hydrogen; dihydrogen peroxide; L-Selectride; sodium tris(acetoxy)borohydride; triethylamine; trifluoroacetic acid; lithium hydroxide; lithium diisopropyl amide;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene;
2: Evan's asymmetric alkylation / 4: Curtius rearrangement;
DOI:10.1016/j.bmcl.2012.01.014
- Guidance literature:
-
Multi-step reaction with 7 steps
1: palladium on activated charcoal; hydrogen / ethanol
2: cis-nitrous acid; potassium iodide / ethanol
3: borane / tetrahydrofuran
4: sodium tris(acetoxy)borohydride / dichloromethane
5: N,N-dimethyl-formamide / 50 - 60 °C
6: trifluoroacetic acid / water
7: L-Selectride / tetrahydrofuran
With
palladium on activated charcoal; borane; hydrogen; cis-nitrous acid; L-Selectride; sodium tris(acetoxy)borohydride; trifluoroacetic acid; potassium iodide;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.01.014
- Guidance literature:
-
Multi-step reaction with 5 steps
1: palladium on activated charcoal; hydrogen / methanol
2: sodium tris(acetoxy)borohydride / dichloromethane
3: N,N-dimethyl-formamide / 50 - 60 °C
4: trifluoroacetic acid / water
5: L-Selectride / tetrahydrofuran
With
palladium on activated charcoal; hydrogen; L-Selectride; sodium tris(acetoxy)borohydride; trifluoroacetic acid;
In
tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2012.01.014