4-methoxycarbonyl-4'-ferrocenylbiphenyl

Base Information

Chemical Name:4-methoxycarbonyl-4'-ferrocenylbiphenyl
CAS No.:1237514-33-8
Molecular Formula:C₂₄H₂₀FeO₂
Molecular Weight:396.269
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-methoxycarbonyl-4'-ferrocenylbiphenyl

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Technology Process of 4-methoxycarbonyl-4'-ferrocenylbiphenyl

There total 1 articles about 4-methoxycarbonyl-4'-ferrocenylbiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: (4-bromophenyl)ferrocene

: 99768-12-4
4-methoxycarbonylphenylboronic acid

: 1237514-33-8
4-methoxycarbonyl-4'-ferrocenylbiphenyl

Guidance literature:: With Pd(P(C₆H₅)3)4; K₂CO₃; In water; N,N-dimethyl-formamide; heating mixt. of ferrocene deriv., boronic acid deriv., palladium compd., DMF, water and K2CO3 at 65°C for 2 under N2; cooling to room temp., addn. of water, extn. (CHCl3), washing with water, drying with Na2SO4, filtration, evapn., recrystn. (hot ethanol/water),elem. anal.;
DOI:10.1021/ja103889f

Reference yield: 87.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 1237514-33-8
4-methoxycarbonyl-4'-ferrocenylbiphenyl

: 1237514-31-6
4-carboxy-4'-ferrocenylbiphenyl

Guidance literature:: With KOH; In methanol; addn. of KOH to methanolic soln. of ferrocene deriv., refluxing for 3 h,cooling to room temp., addn. of aq. HCl and water; isolation of ppt., elem. anal.;
DOI:10.1021/ja103889f