(+/-)-Dispermon

Base Information

• Chemical Name: (+/-)-Dispermon
• CAS No.: 63568-42-3
• Molecular Formula: C₂₀H₂₈O₃
• Molecular Weight: 316.441
• Mol file: 63568-42-3.mol

Synonyms:

Chemical Property of (+/-)-Dispermon

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (+/-)-Dispermon

There total 10 articles about (+/-)-Dispermon which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-Isopropyl-3,4-dimethoxy-phenyl)-methanol (71596-68-4) → (+/-)-Dispermon (51918-95-7,63568-42-3)

Guidance literature:

Multi-step reaction with 7 steps

1: SOCl₂ / diethyl ether

2: naphthalene/Li / tetrahydrofuran

3: Et₃SiH, BF₃-Et₂O / CH₂Cl₂

4: AlCl₃ / benzene / Heating

5: K₂CO₃ / butan-2-one / Heating

6: CrO₃ / acetic acid

7: BBr₃ / CH₂Cl₂

With chromium(VI) oxide; triethylsilane; aluminium trichloride; thionyl chloride; naphthalene; boron trifluoride diethyl etherate; boron tribromide; lithium; potassium carbonate; In tetrahydrofuran; diethyl ether; dichloromethane; acetic acid; butanone; benzene;

DOI:10.1246/bcsj.52.1957

Reference yield:

3,4-Dimethoxy-2-isopropylbenzylchlorid (63512-92-5) → (+/-)-Dispermon (51918-95-7,63568-42-3)

Guidance literature:

Multi-step reaction with 6 steps

1: naphthalene/Li / tetrahydrofuran

2: Et₃SiH, BF₃-Et₂O / CH₂Cl₂

3: AlCl₃ / benzene / Heating

4: K₂CO₃ / butan-2-one / Heating

5: CrO₃ / acetic acid

6: BBr₃ / CH₂Cl₂

With chromium(VI) oxide; triethylsilane; aluminium trichloride; naphthalene; boron trifluoride diethyl etherate; boron tribromide; lithium; potassium carbonate; In tetrahydrofuran; dichloromethane; acetic acid; butanone; benzene;

DOI:10.1246/bcsj.52.1957

Reference yield:

2-Isopropyl-3,4-dimethoxy-1-[2-(2,6,6-trimethyl-cyclohex-1-enyl)-ethyl]-benzene (63512-95-8) → (+/-)-Dispermon (51918-95-7,63568-42-3)

Guidance literature:

Multi-step reaction with 4 steps

1: AlCl₃ / benzene / Heating

2: K₂CO₃ / butan-2-one / Heating

3: CrO₃ / acetic acid

4: BBr₃ / CH₂Cl₂

With chromium(VI) oxide; aluminium trichloride; boron tribromide; potassium carbonate; In dichloromethane; acetic acid; butanone; benzene;

DOI:10.1246/bcsj.52.1957

upstream raw materials:

(4aR,10aR)-8-Isopropyl-6,7-dimethoxy-1,1,4a-trimethyl-2,3,4,4a,10,10a-hexahydro-1H-phenanthren-9-one

(2-Isopropyl-3,4-dimethoxy-phenyl)-methanol

3,4-Dimethoxy-2-isopropylbenzylchlorid

2-Isopropyl-3,4-dimethoxy-1-[2-(2,6,6-trimethyl-cyclohex-1-enyl)-ethyl]-benzene