Pd₂HBr₃(bis(diphenylphosphino)methane)2

Base Information

• Chemical Name: Pd₂HBr₃(bis(diphenylphosphino)methane)2
• CAS No.: 650604-43-6
• Molecular Formula: C₅₀H₄₅Br₃P₄Pd₂
• Molecular Weight: 1222.35
• Mol file: 650604-43-6.mol

Synonyms:

Chemical Property of Pd₂HBr₃(bis(diphenylphosphino)methane)2

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Pd₂HBr₃(bis(diphenylphosphino)methane)2

There total 1 articles about Pd₂HBr₃(bis(diphenylphosphino)methane)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

Pd2Br2(μ-bis(diphenylphosphino)methane)2 (60482-68-0) + hydrogen bromide (10035-10-6,12258-64-9) → Pd2HBr3(bis(diphenylphosphino)methane)2 (650604-43-6)

Guidance literature:

In dichloromethane; water; under inert atm. aq. HBr was added to soln. Pd2Br2(dppm)2 in CH2Cl2 and stirred for 5 min; CH2Cl2 layer was separated, solvent was removed in vacuo; elem. anal.;

DOI:10.1016/j.jorganchem.2003.09.017

Reference yield:

Pd2HBr3(bis(diphenylphosphino)methane)2 (650604-43-6) → Pd2Br2(μ-bis(diphenylphosphino)methane)2 (60482-68-0) + PdBr2(bis(diphenylphosphino)methane) (77462-41-0)

Guidance literature:

In dichloromethane-d2; 24 h; identified by NMR;

DOI:10.1016/j.jorganchem.2003.09.017

upstream raw materials:

Pd2Br2(μ-bis(diphenylphosphino)methane)2

hydrogen bromide

Downstream raw materials:

Pd2Br2(μ-bis(diphenylphosphino)methane)2

PdBr₂(bis(diphenylphosphino)methane)