1-Cycloheptene-1-carboxaldehyde, 2-(phenylethynyl)-

Base Information

Chemical Name:1-Cycloheptene-1-carboxaldehyde, 2-(phenylethynyl)-
CAS No.:106180-32-9
Molecular Formula:C16H16O
Molecular Weight:224.302
Hs Code.:
DSSTox Substance ID:DTXSID90457983
Nikkaji Number:J2.068.905F

Synonyms:1-Cycloheptene-1-carboxaldehyde, 2-(phenylethynyl)-;106180-32-9;DTXSID90457983;2-(Phenylethynyl)-1-cycloheptene-1-carbaldehyde

Suppliers and Price of 1-Cycloheptene-1-carboxaldehyde, 2-(phenylethynyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Cycloheptene-1-carboxaldehyde, 2-(phenylethynyl)-

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:224.120115130
Heavy Atom Count:17
Complexity:358

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(=C(CC1)C#CC2=CC=CC=C2)C=O

Technology Process of 1-Cycloheptene-1-carboxaldehyde, 2-(phenylethynyl)-

There total 7 articles about 1-Cycloheptene-1-carboxaldehyde, 2-(phenylethynyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 85236-13-1
2-bromocyclohept-1-ene-1-carbaldehyde

: 536-74-3
phenylacetylene

: 106180-32-9
2-Phenylethynyl-cyclohept-1-enecarbaldehyde

Guidance literature:: With copper(l) iodide; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(97)01393-2

Reference yield:

: 502-42-1
cycloheptanone

: 106180-32-9
2-Phenylethynyl-cyclohept-1-enecarbaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / PBr₃ / CHCl₃

2: 73 percent / CuI, NEt₃ / Pd(PPh₃)4 / dimethylformamide

With copper(l) iodide; phosphorus tribromide; triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In chloroform; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(97)01393-2