Technology Process of Oxiranecarbonitrile, 3-(2-ethynyl-1-cyclohepten-1-yl)-2-phenyl-, cis-
There total 5 articles about Oxiranecarbonitrile, 3-(2-ethynyl-1-cyclohepten-1-yl)-2-phenyl-, cis- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium tert-butylate;
In
tert-butyl alcohol; benzene;
for 80h;
Ambient temperature;
DOI:10.1016/S0040-4020(01)90602-7
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 81 percent / p-toluenesulfonic acid / benzene / 5 h / Heating
2: lithium acetylide-ethylenediamine complex / tetrahydrofuran / 30 - 35 °C
3: 2N H2SO4 / ethanol / 3 h / Ambient temperature
4: 59 percent / potassium t-butoxide / 2-methyl-propan-2-ol; benzene / 80 h / Ambient temperature
With
sulfuric acid; potassium tert-butylate; lithium acetylide-ethylenediamine complex; toluene-4-sulfonic acid;
In
tetrahydrofuran; ethanol; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4020(01)90602-7
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium acetylide-ethylenediamine complex / tetrahydrofuran / 30 - 35 °C
2: 2N H2SO4 / ethanol / 3 h / Ambient temperature
3: 59 percent / potassium t-butoxide / 2-methyl-propan-2-ol; benzene / 80 h / Ambient temperature
With
sulfuric acid; potassium tert-butylate; lithium acetylide-ethylenediamine complex;
In
tetrahydrofuran; ethanol; tert-butyl alcohol; benzene;
DOI:10.1016/S0040-4020(01)90602-7
